ChemicalBook--->CAS DataBase List--->24214-73-1

24214-73-1

24214-73-1 Structure

24214-73-1 Structure
IdentificationMore
[Name]

CYCLOHEXYLHYDRAZINE HYDROCHLORIDE
[CAS]

24214-73-1
[Synonyms]

1-CYCLOHEXYLHYDRAZINE HYDROCHLORIDE
CYCLOHEXYLHYDRAZINE HYDROCHLORIDE
CyclohexylhydrazineHCl
[Molecular Formula]

C6H15ClN2
[MDL Number]

MFCD00060160
[Molecular Weight]

150.65
[MOL File]

24214-73-1.mol
Chemical PropertiesBack Directory
[Melting point ]

110-114 °C(lit.)
[storage temp. ]

Keep in dark place,Inert atmosphere,2-8°C
[form ]

Crystalline Powder
[color ]

White
[Water Solubility ]

almost transparency
[InChI]

InChI=1S/C6H14N2.ClH/c7-8-6-4-2-1-3-5-6;/h6,8H,1-5,7H2;1H
[InChIKey]

JZRHODNPRNTXKO-UHFFFAOYSA-N
[SMILES]

C1(NN)CCCCC1.Cl
[CAS DataBase Reference]

24214-73-1(CAS DataBase Reference)
Safety DataBack Directory
[Symbol(GHS) ]

Exclamation Mark (GHS07)Corrosion (GHS05)
GHS07,GHS05
[Signal word ]

Danger
[Hazard statements ]

H302+H312+H332-H315-H319-H314
[Precautionary statements ]

P280-P305+P351+P338-P310-P261-P264-P270-P271-P301+P312+P330-P302+P352+P312+P362+P364-P304+P340+P312-P305+P351+P338+P337+P313-P501
[Hazard Codes ]

C
[Risk Statements ]

R34:Causes burns.
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
[RIDADR ]

UN 3263 8/PG 2
[WGK Germany ]

3
[HazardClass ]

8
[PackingGroup ]

Ⅱ
[HS Code ]

29280000
[Storage Class]

8A - Combustible corrosive hazardous materials
[Hazard Classifications]

Skin Corr. 1B
Hazard InformationBack Directory
[Chemical Properties]

White to light yellow powder,crystals or
[Synthesis]

TERT-BUTYL 2-CYCLOHEXYLHYDRAZINECARBOXYLATE

60295-21-8

Cyclohexylhydrazine hydrochloride

24214-73-1

GENERAL METHOD: tert-Butyl 2-cyclohexylhydrazine-1-carboxylate (1.9 g, 8.87 mmol) was dissolved in dioxane and to this solution was added a dioxane solution (20 mL) of 4 M HCl. The reaction mixture was heated to reflux and stirred overnight. Upon completion of the reaction, it was cooled to room temperature, the precipitated white precipitate was collected by filtration, washed with a small amount of cold dioxane and dried to give cyclohexylhydrazine hydrochloride (1.8 g, yield: >100%) as a white solid.

[References]

[1] Patent: WO2016/123392, 2016, A2. Location in patent: Paragraph 00476
[2] Patent: WO2014/82598, 2014, A1. Location in patent: Paragraph 0419
[3] Journal of Organic Chemistry, 1981, vol. 46, # 26, p. 5413 - 5414
[4] Patent: WO2005/40169, 2005, A2. Location in patent: Page/Page column 150
Spectrum DetailBack Directory
[Spectrum Detail]

Cyclohexylhydrazine hydrochloride(24214-73-1)1HNMR
Cyclohexylhydrazine hydrochloride(24214-73-1)IR1
Cyclohexylhydrazine hydrochloride(24214-73-1)IR2
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

24214-73-1(sigmaaldrich)
[TCI AMERICA]

Cyclohexylhydrazine Hydrochloride,>98.0%(T)(24214-73-1)
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