| Identification | Back Directory | [Name]
6-Bromoquinazolin-4-ol | [CAS]
32084-59-6 | [Synonyms]
CHEMBRDG-BB 4002728
6-BROMO-4-QUINAZOLONE
6-Bromo-4-quinazolinol
6-Bromoquinazolin-4-ol
6-bromo-4-quinazolinone
6-Bromoquinazolin-4(3H)-one
6-bromo-4(3h)-quinazolinone
6-BROMO-3H-QUINAZOLIN-4-ONE
6-Bromo-4-hydroxyquinazoline
4(3H)-Quinazolinone, 6-broMo-
6-Bromoquinazolin-4(3H)-one 98%
6-Bromo-4-hydroxyquinazoline >
6-Bromo-1,4-dihydroquinazolin-4-one
6-broMo-3,4-dihydroquinazolin-4-one
6-Bromo-3,4-dihydro-4-oxoquinazoline
6-Bromo-3,4-dihydro-4-oxoquinazoline 98%
6-Bromoquinazolin-4-ol ISO 9001：2015 REACH
6-bromoquinazolin-4(3H)-one(SALTDATA: FREE) | [Molecular Formula]
C8H5BrN2O | [MDL Number]
MFCD01219541 | [MOL File]
32084-59-6.mol | [Molecular Weight]
225.04 |
| Chemical Properties | Back Directory | [Melting point ]
131-132 °C | [Boiling point ]
374.2±44.0 °C(Predicted) | [density ]
1.82±0.1 g/cm3(Predicted) | [storage temp. ]
Keep in dark place,Inert atmosphere,Room temperature | [form ]
powder to crystal | [pka]
1.05±0.20(Predicted) | [color ]
White to Orange to Green | [InChI]
InChI=1S/C8H5BrN2O/c9-5-1-2-7-6(3-5)8(12)11-4-10-7/h1-4H,(H,10,11,12) | [InChIKey]
OVEISJPVPHWEHR-UHFFFAOYSA-N | [SMILES]
N1C2=C(C=C(Br)C=C2)C(=O)NC=1 |
| Hazard Information | Back Directory | [Chemical Properties]
White powder | [Synthesis]
In a 10 mL microwave reaction tube, 5-bromo-2-iodobenzoic acid (1.0 mmol), formamidine hydrochloride (1.2 mmol), CuCl2 (0.1 mmol), ligand L2 (0.1 mmol), and NaOH (4.0 equiv) were sequentially added, followed by 3.0 mL of deionized water. The reaction tube was sealed with a septum and placed in a microwave reactor. Using a CEM Discover microwave synthesizer, radiation was applied at 120 W for 20 min at room temperature, and continuous stirring was maintained during the reaction. After completion of the reaction, the solvent was removed by distillation under reduced pressure. The crude product was purified by silica gel column chromatography to afford the target compound 6-bromoquinoxalin-4-ol. The structures of all the products were confirmed by nuclear magnetic resonance (NMR) and mass spectrometry (MS) analysis. | [References]
[1] Synthetic Communications, 2018, vol. 48, # 24, p. 3089 - 3098 |
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Shangchem Co., Ltd.
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