| Identification | Back Directory | [Name]
Acetamide, N-(2-fluoro-4-methylphenyl)- | [CAS]
326-67-0 | [Synonyms]
N-(2-fluoro-4-methylphenyl)acetamide
Acetamide, N-(2-fluoro-4-methylphenyl)- | [Molecular Formula]
C9H10FNO | [MOL File]
326-67-0.mol | [Molecular Weight]
167.18 |
| Hazard Information | Back Directory | [Synthesis]
To a solution of 2-fluoro-4-methylaniline (250 g, 2 mol) and triethylamine (202 g, 2 mol) dissolved in 2 L of dichloromethane, acetyl chloride (156 g, 2 mol) was added slowly and dropwise. The reaction mixture was stirred at 0 °C for 2 h and subsequently washed with dilute hydrochloric acid. The organic phase was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude intermediate N-(2-fluoro-4-methylphenyl)acetamide (334 g, 87% yield). | [References]
[1] Patent: WO2010/100189, 2010, A1. Location in patent: Page/Page column 70
[2] Patent: WO2013/30262, 2013, A1. Location in patent: Page/Page column 51
[3] Patent: WO2013/30319, 2013, A2. Location in patent: Page/Page column 45
[4] Patent: WO2013/30338, 2013, A2. Location in patent: Page/Page column 60 |
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