ChemicalBook--->CAS DataBase List--->3283-07-6

3283-07-6

Request For Quotation
3283-07-6 Structure

3283-07-6 Structure
IdentificationBack Directory
[Name]

N,N,N',N'-Tetrakis(4-aminophenyl)-1,4-benzenediamine
[CAS]

3283-07-6
[Synonyms]

TPDA
Tetrakis Phenylenediamine
N,N,N',N'-Tetrakis(4-aminophenyl)-1,4-p
N,N,N',N'-Tetra(p-aminophenyl)-p-phenylenediamine
4,4',4'',4'''-(p-Phenylenebisnitrilo)tetrakisaniline
N,N,N',N'-Tetrakis(4-aminophenyl)-p-phenylenediamine
n,n,n',n'-tetrakis(p-aminophenyl)-p-phenylenediamine
n,n,n',n'-tetrakis(4-aminophenyl)-1,4-benzenediamine
N,N,N,N-Tetrakis-(4-amino-phenyl)-benzene-1,4-diamine
N,N,N',N'-TETRAKIS(4-AMINOPHENYL)-1,4-PHENYLENEDIAMINE
1,4-Benzenediamine, N,N,N',N'-tetrakis(4-aminophenyl)-
1,4-BenzenediaMine,N1,N1,N4,N4-tetrakis(4-aMinophenyl)-
4,4',4'',4'''-[(1,4-Phenylene)bisnitrilo]tetrakisaniline
4,4',4'',4'''-(1,4-Phenylene)bis(nitrilo)tetrakisaniline
N,N,N',N'-Tetrakis(4-aminophenyl)-1,4-phenylenediamine 98%
N,N,N',N'-Tetrakis(4-aminophenyl)-1,4-benzenediamine
N1,N1'-(1,4-phenylene)bis(N1-(4-aminophenyl)benzene-1,4-diamine)
4-N-[4-(4-amino-N-(4-aminophenyl)anilino)phenyl]-4-N-(4-aminophenyl)benzene-1,4-diamine
[Molecular Formula]

C30H28N6
[MDL Number]

MFCD06657652
[MOL File]

3283-07-6.mol
[Molecular Weight]

472.58
Chemical PropertiesBack Directory
[Melting point ]

>300°C
[Boiling point ]

765.6±60.0 °C(Predicted)
[density ]

1.309
[storage temp. ]

Keep in dark place,Inert atmosphere,Room temperature
[solubility ]

Soluble in DMSO, DMF Insoluble in methanol & water
[pka]

6.85±0.10(Predicted)
[color ]

Greenish grey colored crystalline powder
[InChI]

InChI=1S/C30H28N6/c31-21-1-9-25(10-2-21)35(26-11-3-22(32)4-12-26)29-17-19-30(20-18-29)36(27-13-5-23(33)6-14-27)28-15-7-24(34)8-16-28/h1-20H,31-34H2
[InChIKey]

LVPYYSKDNVAARK-UHFFFAOYSA-N
[SMILES]

C1(N(C2=CC=C(N)C=C2)C2=CC=C(N)C=C2)=CC=C(N(C2=CC=C(N)C=C2)C2=CC=C(N)C=C2)C=C1
[EPA Substance Registry System]

1,4-Benzenediamine, N,N,N',N'-tetrakis(4-aminophenyl)- (3283-07-6)
Safety DataBack Directory
[Symbol(GHS) ]

Exclamation Mark (GHS07)
GHS07
[Signal word ]

Warning
[Hazard statements ]

H302
[Precautionary statements ]

P280-P305+P351+P338
[Risk Statements ]

20/21/22
[Safety Statements ]

22-36/37/39
[TSCA ]

TSCA listed
[HS Code ]

2921599090
Hazard InformationBack Directory
[Uses]

N,N,N'',N''-Tetrakis(4-aminophenyl)-1,4-phenylenediamine can be used as composition and solution for temporary bonding.
[Synthesis]

N,N,N',N'-Tetrakis(4-nitrophenyl)-p-phenylenediamine

3283-05-4

N,N,N',N'-Tetrakis(4-aminophenyl)-1,4-benzenediamine

3283-07-6

Example 4: Preparation of compound (III-1) 160 g of N,N,N',N'-tetrakis(p-nitrophenyl)p-phenylenediamine (II-1), 1.07 g of ferric chloride (III) hexahydrate, 1.55 g of iron (III) oxide, 16.2 g of activated carbon and 1400 ml of 1 -methyl-2-pyrrolidinone were added into a three-necked flask and heated under stirring to an internal temperature of 100 °C. Subsequently, 450 g of 80% hydrazine monohydrate aqueous solution was slowly added dropwise, the reaction temperature was maintained in the range of 100-110 °C, and the reaction was continuously stirred for 5 hours. Upon completion of the reaction, it was cooled to room temperature. The reaction mixture was filtered to remove the activated carbon, followed by the sequential dropwise addition of 800 ml of methanol and 1200 ml of water to the filtrate, and the precipitated crystals were collected by filtration by pumping to afford 126.3 g of N1,N1'-(1,4-phenylene)bis(N1-(4-aminophenyl)benzene-1,4-diamine (III-1) in 99% yield. Spectral analysis of the product showed M/e = 472.

[References]

[1] Patent: WO2007/73000, 2007, A1. Location in patent: Page/Page column 33
[2] Patent: EP1767587, 2007, A2. Location in patent: Page/Page column 15
[3] Patent: WO2007/73000, 2007, A1. Location in patent: Page/Page column 31-32
[4] Patent: WO2007/73000, 2007, A1. Location in patent: Page/Page column 32
[5] Patent: WO2007/73000, 2007, A1. Location in patent: Page/Page column 32-33
Spectrum DetailBack Directory
[Spectrum Detail]

N,N,N',N'-Tetrakis(4-aminophenyl)-1,4-benzenediamine(3283-07-6)1HNMR
3283-07-6 suppliers list
Company Name: Shanghai Baisley Pharmaceutical Technology Co., Ltd.  Gold
Telephone: 021-15995002467 15995002467
Website: www.besleychem.com/
Company Name: Beijing HwrkChemical Technology Co., Ltd  
Telephone: 89508211 18501085097
Website: www.hwrkchemical.com
Company Name: BeiJing Hwrk Chemicals Limted  
Telephone: 0757-86329057 18934348241
Website: www.hwrkchemical.com/
Company Name: Energy Chemical  
Telephone: 400-0056266
Website: www.energy-chemical.com
Company Name: HANSHANG CHEMICAL SCIENTIFIC LIMITED  
Telephone: 021-50521775 15800962688
Website: http://www.hanshangchem.com
Company Name: Shanghai Sunway Pharmaceutical Technology Co., Ltd  
Telephone: 13761987713
Website: www.sunwaypharm.cn
Company Name: Beijing Taiya Jie Technology Development Co., Ltd.  
Telephone: 021-33690831-8001 13552411790;18616022633
Website: http://www.tyj-chem.com/
Company Name: Spectrum Chemical Manufacturing Corp.  
Telephone: 021-021-021-67601398-809-809-809 15221380277
Website: www.spectrumchemical.com/oa_html/index.jsp?minisite=10020&respid=22372&language=us
Company Name: ShangHai D&B Biological Science and Technology Co.Ltd  
Telephone: 400-008-9730,021-54359730 400-008-9730
Website: http://www.chemxyz.cn
Company Name: Finetech Industry Limited  
Telephone: 027-87465837 19945049750
Website: https://www.finetechchem.com/
Company Name: Shanghai Macklin Biochemical Co.,Ltd.  
Telephone: 15221275939 15221275939
Website: www.macklin.cn
Company Name: Shanghai Na Qian Chemical Technology Co. Ltd.  
Telephone: 13598610367 13598610367
Website: https://www.chemicalbook.com/supplier/11167012/
Company Name: Nanjing Chalf-Pharm Technology Co., Ltd.  
Telephone: 025-57018978 18251899859
Website: http://www.chalf-pharm.com
Company Name: Mascot I.E. Co., Ltd  
Telephone: 0519-85010339 13584504415
Website: http://www.mascot-ie.com/
Company Name: Shanghai KaiYuLin pharmaceutical technology co., LTD  
Telephone: 021-18721936-595 18721936595
Website: http://www.kylpharm.com
Company Name: Chizhou Kailong Import and Export Trade Co., Ltd.  
Telephone:
Website: www.chemicalbook.com/ShowSupplierProductsList16778/0_EN.htm
Company Name: Shanghai Mixiu Chemical Co., Ltd.  
Telephone: 18101936766
Website: http://www.shmychem.com
Company Name: Shanghai Uchem Inc.  
Telephone: 15618758386 15618758386
Website: https://www.chemicalbook.com/ShowSupplierProductsList15300/0_EN.htm
Tags:3283-07-6 Related Product Information
150-77-6 2146095-56-7 2097565-50-7 15546-43-7 1630723-98-6 865448-72-2 106-50-3