| Identification | Back Directory | [Name]
BUTTPARK 91\15-77 | [CAS]
34598-50-0 | [Synonyms]
BUTTPARK 91\15-77
5-BROMO-1-INDANOL
5-BROMOINDAN-1-OL
5-broMo-2,3-dihydro-1H-inden-1-ol
1H-Inden-1-ol, 5-bromo-2,3-dihydro- | [EINECS(EC#)]
604-604-1 | [Molecular Formula]
C9H9BrO | [MDL Number]
MFCD06808667 | [MOL File]
34598-50-0.mol | [Molecular Weight]
213.07 |
| Chemical Properties | Back Directory | [Melting point ]
77-79 °C(Solv: hexane (110-54-3)) | [Boiling point ]
307.7±37.0 °C(Predicted) | [density ]
1.617±0.06 g/cm3(Predicted) | [storage temp. ]
2-8°C | [pka]
14.05±0.20(Predicted) | [Appearance]
White to off-white Solid | [InChI]
InChI=1S/C9H9BrO/c10-7-2-3-8-6(5-7)1-4-9(8)11/h2-3,5,9,11H,1,4H2 | [InChIKey]
DRXIUUZVRAOHBS-UHFFFAOYSA-N | [SMILES]
C1(O)C2=C(C=C(Br)C=C2)CC1 |
| Hazard Information | Back Directory | [Synthesis]
A mixture of 5-bromo-2, 3-dihydroinden-1-one, and NaBH4 in EtOH was stirred at 60° C for 6 minutes. After evaporation of the solvent, the residue was purified by chromatography (silica gel; 1:2 EtOAc/hexane), providing compound 47.2 in 100% yield.
| [References]
[1] Bioorganic and Medicinal Chemistry Letters, 2002, vol. 12, # 5, p. 827 - 832
[2] Patent: US2007/66647, 2007, A1. Location in patent: Page/Page column 69
[3] ACS Medicinal Chemistry Letters, 2010, vol. 1, # 9, p. 483 - 487
[4] Patent: WO2009/39134, 2009, A1. Location in patent: Page/Page column 186-187
[5] Patent: WO2006/63179, 2006, A1. Location in patent: Page/Page column 48 |
|
| Company Name: |
Tetranov Biopharm
|
| Telephone: |
13526569071 |
| Website: |
http://www.leadmedpharm.com/index.html |
| Company Name: |
Wuxi AppTec
|
| Telephone: |
022-59987777 13552403979 |
| Website: |
www.labnetwork.com |
|