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3561-67-9

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3561-67-9 Structure

3561-67-9 Structure
IdentificationMore
[Name]

BIS(PHENYLTHIO)METHANE
[CAS]

3561-67-9
[Synonyms]

1,1'-(METHYLENEBIS(THIO))BISBENZENE
1-([(PHENYLTHIO)METHYL]THIO)BENZENE
BIS(PHENYLTHIO)METHANE
DIPHENYLTHIOMETHANE
FORMALDEHYDE DIPHENYL MERCAPTAL
([(Phenylsulfanyl)methyl]sulfanyl)benzene
Benzene, 1,1'-[methylenebis(thio)]bis-
Bis(phenyithio)methane
Bis(thiophenoxy)methane
[methylenebis(thio)]bisbenzene
Formaldehydediphenylmercapatal
Bis(phenylthio)methane,98+%
Diphenylthiomethane, Formaldehyde diphenyl mercaptal
Methylenebis(phenyl sulfide)
Phenyl(phenylthiomethyl) sulfide
[EINECS(EC#)]

222-624-4
[Molecular Formula]

C13H12S2
[MDL Number]

MFCD00003067
[Molecular Weight]

232.36
[MOL File]

3561-67-9.mol
Chemical PropertiesBack Directory
[Appearance]

light yellow crystalline powder
[Melting point ]

34-37 °C(lit.)
[Boiling point ]

194 °C8 mm Hg(lit.)
[density ]

1.2633 (rough estimate)
[refractive index ]

1.6210 (estimate)
[Fp ]

>230 °F
[storage temp. ]

Sealed in dry,Room Temperature
[form ]

powder to crystal
[color ]

White to Light yellow
[Water Solubility ]

Insoluble in water.
[BRN ]

1874146
[InChI]

1S/C13H12S2/c1-3-7-12(8-4-1)14-11-15-13-9-5-2-6-10-13/h1-10H,11H2
[InChIKey]

ZHUPZVIALZHGGP-UHFFFAOYSA-N
[SMILES]

C(Sc1ccccc1)Sc2ccccc2
[CAS DataBase Reference]

3561-67-9(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[RIDADR ]

UN 3335
[WGK Germany ]

3
[F ]

13
[HazardClass ]

STENCH
[HS Code ]

29309090
[Storage Class]

11 - Combustible Solids
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Thiophenol-->Diiodomethane-->Sodium thiophenoxide
[Preparation Products]

7-Tridecanol-->Biphenyl-4,4'-dithiol
Hazard InformationBack Directory
[Chemical Properties]

light yellow crystalline powder
[Uses]

Bis(phenylthio)methane (PhSCH2SPh) may be used in the synthesis of the following:
  • dihydroxy thioethers
  • [Cu4I4{μ-PhS2CH2SPh}2]n
  • [(η5-C5Me5)MCl2(η1-(PhS)2CH2)] (M=Rh, Ir ; C5Me5= pentamethylcyclopentadienyl)
  • 6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactoheptodialdo-1,5-pyranose diphenyl dithioacetal
[Synthesis Reference(s)]

Synthetic Communications, 19, p. 31, 1989 DOI: 10.1080/00397918908050949
Synthesis, p. 447, 1975 DOI: 10.1055/s-1975-23797
[General Description]

Bis(phenylthio)methane (PhSCH2SPh) is a dithioether ligand. It forms coordination complex with silver(I) salts. It participates in the synthesis of (-)-rasfonin.
Spectrum DetailBack Directory
[Spectrum Detail]

BIS(PHENYLTHIO)METHANE(3561-67-9)MS
BIS(PHENYLTHIO)METHANE(3561-67-9)1HNMR
BIS(PHENYLTHIO)METHANE(3561-67-9)13CNMR
BIS(PHENYLTHIO)METHANE(3561-67-9)IR1
BIS(PHENYLTHIO)METHANE(3561-67-9)IR2
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

Bis(phenylthio)methane, 97%(3561-67-9)
[Alfa Aesar]

Bis(phenylthio)methane, 98+%(3561-67-9)
[Sigma Aldrich]

3561-67-9(sigmaaldrich)
[TCI AMERICA]

Bis(phenylthio)methane,>97.0%(GC)(3561-67-9)
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