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525-03-1

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525-03-1 Structure

525-03-1 Structure
IdentificationMore
[Name]

9H-FLUOREN-9-AMINE
[CAS]

525-03-1
[Synonyms]

9-AMINOFLUORENE
9H-FLUOREN-9-AMINE
FLUOREN-9-AMINE
TIMTEC-BB SBB005783
Fluoren-9-ylamine
9-AMINOFLUOROENE
9-Amino-9H-fluorene
[Molecular Formula]

C13H11N
[MDL Number]

MFCD00871339
[Molecular Weight]

181.23
[MOL File]

525-03-1.mol
Chemical PropertiesBack Directory
[Melting point ]

64℃
[Boiling point ]

304.35°C (rough estimate)
[density ]

1.162
[refractive index ]

1.6118 (estimate)
[storage temp. ]

under inert gas (nitrogen or Argon) at 2–8 °C
[pka]

8.18±0.20(Predicted)
[CAS DataBase Reference]

525-03-1(CAS DataBase Reference)
Hazard InformationBack Directory
[Synthesis Reference(s)]

Journal of Medicinal Chemistry, 23, p. 184, 1980 DOI: 10.1021/jm00176a015
[Purification Methods]

Purify it by converting it to the hydrochloride with HCl, then basify it with NH3 and recrystallise it from pet ether (m 62-63o) or from hexane. The hydrochloride M 217.7, m ~255o(dec, from EtOH). [Ingold et al. J Chem Soc 1493 1933, Mathieu Bull Soc Chim Fr 1526 1971, Beilstein 12 H 1331, 12 I 553, 12 II 780, 1 2 III 3297, 12 IV 3390.]
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