ChemicalBook--->CAS DataBase List--->57963-08-3

57963-08-3

57963-08-3 Structure

57963-08-3 Structure
IdentificationBack Directory
[Name]

2-AMINO-5,6-DIMETHYLPYRIDINE
[CAS]

57963-08-3
[Synonyms]

NSC 95996
6-AMino-2,3-lutidine
5,6-diMethyl-2-PyridinaMine
5,6-dimethylpyridin-2-amine
2-amino-5,6-dimethylpyridin
5,6-Dimethyl-2-aminopyridine
6-Amino-2,3-dimethylpyridine
2-AMINO-5,6-DIMETHYLPYRIDINE
2-Pyridinamine,5,6-dimethyl-
2-Amino-5,6-dimenthylpyridine
(5,6-dimethyl-2-pyridyl)amine
5,6-DIMETHYL-PYRIDIN-2-YLAMINE
5,6-Dimethylpyridin-2-amine, 2-Amino-5,6-dimethylpyridine, 6-Amino-2,3-lutidine
[Molecular Formula]

C7H10N2
[MDL Number]

MFCD06200777
[MOL File]

57963-08-3.mol
[Molecular Weight]

122.17
Chemical PropertiesBack Directory
[Appearance]

Light Yellow Low-Melting Solid
[storage temp. ]

Keep in dark place,Inert atmosphere,2-8°C
[solubility ]

Chloroform, Dichloromethane
[form ]

Solid
[color ]

Light Yellow
[InChI]

InChI=1S/C7H10N2/c1-5-3-4-7(8)9-6(5)2/h3-4H,1-2H3,(H2,8,9)
[InChIKey]

UZAOIPZZPZCFES-UHFFFAOYSA-N
[SMILES]

C1(N)=NC(C)=C(C)C=C1
[CAS DataBase Reference]

57963-08-3
Hazard InformationBack Directory
[Chemical Properties]

Light Yellow Low-Melting Solid
[Synthesis]

A mixture of 2-amino-5-bromo-6-methylpyridine (561 mg, 3.0 mmol), K2CO3 (1.24 g, 9.0 mmol) and Pd(dppf)Cl2·CH2Cl2 (245 mg, 0.30 mmol) was added to a solution of trimethylboroxine (377 mg, 3.0 mmol) in water (1 mL) and dioxane (10 mL). The mixture was heated at reflux for 3 h. After cooling to rt, the mixture was poured into water (50 mL). The mixture was extracted with diethyl ether (3*50ml), and the combined organic phases were dried (Na2SO4) and concentrated. Purification by chromatography (EtOAc/heptane) gave 5,6-Dimethylpyridin-2-amine as a black-brown solid. Yield: 67 %.
Safety DataBack Directory
[Symbol(GHS) ]


GHS07
[Signal word ]

Warning
[Hazard statements ]

H302-H315-H319-H335
[Precautionary statements ]

P261-P305+P351+P338
[Hazard Codes ]

Xi,Xn
[Risk Statements ]

36/37/38-41-37/38-22
[Safety Statements ]

26-37/39-39
[HS Code ]

29339990
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