ChemicalBook--->CAS DataBase List--->59528-27-7

59528-27-7

59528-27-7 Structure

59528-27-7 Structure
IdentificationMore
[Name]

4-Iodobenzylamine hydrochloride
[CAS]

59528-27-7
[Synonyms]

4-IODOBENZYLAMINE HCL
4-IODOBENZYLAMINE HYDROCHLORIDE
4-IODOBENZYLAMINE, HYDROCHLORIDE SALT
[EINECS(EC#)]

-0
[Molecular Formula]

C7H9ClIN
[MDL Number]

MFCD04039324
[Molecular Weight]

269.51
[MOL File]

59528-27-7.mol
Chemical PropertiesBack Directory
[Melting point ]

299-303 °C(lit.)
[storage temp. ]

Keep in dark place,Inert atmosphere,Room temperature
[Appearance]

White to off-white Powder
[Water Solubility ]

Soluble in water.
[Sensitive ]

Light Sensitive
[BRN ]

3691299
[CAS DataBase Reference]

59528-27-7(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S22:Do not breathe dust .
S24/25:Avoid contact with skin and eyes .
[WGK Germany ]

3
[Hazard Note ]

Irritant/Light Sensitive
[HS Code ]

29214990
Hazard InformationBack Directory
[Uses]

4-Iodobenzylamine hydrochloride is used to prepare cyclic amide by reacting with methyl 4-bromomethyl-3-methoxycarbonylcinnamate in the presence of triethylamine. It is also used in pharmaceuticals, agrochemicals and dye industries.
[General Description]

4-Iodobenzylamine hydrochloride can be synthesized in three steps from 4-iodobenzoic acid.
[Synthesis]

To a suspension of 4-iodobenzamide (11 g, 45 mmol) in THF (50 mL) was added BH3-THF (1M, 22.5 mL, ). 22.5 mmol). The resulting solution was heated to reflux overnight. The reaction was cooled in an ice bath and MeOH-HCl (60 mL) was added slowly and dropwi
Spectrum DetailBack Directory
[Spectrum Detail]

4-Iodobenzylamine hydrochloride(59528-27-7)1HNMR
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

4-Iodobenzylamine hydrochloride, 97%(59528-27-7)
[Sigma Aldrich]

59528-27-7(sigmaaldrich)
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