| Identification | More | [Name]
2,4-Dichlorophenylacetonitrile | [CAS]
6306-60-1 | [Synonyms]
2,4-DCCN
2,4-DICHLOROBENZYL CYANIDE
2,4-DICHLOROPHENYLACETONITRILE
2-(2,4-Dichlorophenyl)acetonitrile
2,4-Dichlorobenzeneacetonitrile
Acetonitrile, (2,4-dichlorophenyl)-
2,4-dichloro cyanobenzene
2,4-Dichlorophenylacetonitrile,98%
(2,4-Dichlorphenyl)acetonitril
2,4-DICHLOROPHENYLACETONITRILE/2,4-DICHLOROBENZYL CYANIDE
11) 2,4-DI CHLORO BENZYL CYANIDE
Benzeneacetonitrile, 2,4-dichloro-
2,4-DICHLOROPHENYLACETONITRILE, 99+% | [EINECS(EC#)]
228-621-4 | [Molecular Formula]
C8H5Cl2N | [MDL Number]
MFCD00001899 | [Molecular Weight]
186.04 | [MOL File]
6306-60-1.mol |
| Safety Data | Back Directory | [Symbol(GHS) ]
GHS07 | [Signal word ]
Warning | [Hazard statements ]
H315-H319-H335 | [Precautionary statements ]
P261-P264-P271-P280-P302+P352-P305+P351+P338 | [Hazard Codes ]
Xi,Xn | [Risk Statements ]
R36/37/38:Irritating to eyes, respiratory system and skin .
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed . | [Safety Statements ]
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection . | [RIDADR ]
3276 | [WGK Germany ]
1
| [HazardClass ]
6.1 | [PackingGroup ]
III | [HS Code ]
29269090 |
| Hazard Information | Back Directory | [Chemical Properties]
white to light yellow crystal powder | [Uses]
2,4-Dichlorophenylacetonitrile was used in the synthesis of 2,4-dichloromandelic acid. | [Synthesis]
General method: 2,4-dichlorobenzyl chloride (1.0 mmol) was mixed with sodium cyanide (2 mmol) in deionized water (5 mL) and polyethylene glycol modified diisocyanate (PEG-MDIL, 0.2 g) was added. The reaction suspension was placed under reflux conditions and the reaction mixture was stirred using a magnetic stirrer for the reaction time referred to in Table 2.After completion of the reaction, the mixture was extracted with ether (2 × 10 mL). The organic extracts were combined, dried with anhydrous calcium chloride and subsequently concentrated under reduced pressure. By this method, the target product 2,4-dichlorophenylacetonitrile was obtained in good to excellent isolated yields (see Scheme 3). | [References]
[1] Organic Preparations and Procedures International, 2011, vol. 43, # 3, p. 285 - 291
[2] Journal of Molecular Liquids, 2015, vol. 202, p. 34 - 39
[3] Journal of Molecular Catalysis A: Chemical, 2012, vol. 365, p. 80 - 86
[4] Applied Organometallic Chemistry, 2018, vol. 32, # 2,
[5] Catalysis Communications, 2012, vol. 18, p. 102 - 105 |
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