869-29-4

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869-29-4 Structure

Identification	More
[Name] ALLYLIDENE DIACETATE
[CAS] 869-29-4
[Synonyms] SD-345 shell345 Shell 345 diacetoxy shellsd345 Shell SD 345 SD 345 (Ester) Diacetoxypropene allylideneacetate crolein diacetate ACROLEIN DIACETATE Allylidene acetate 3,3-Diacetoxypropene ALLYLIDENE DIACETATE 2-Propentyl diacetate 1,1-Diacetoxypropene-2 ,3-Diacetoxy-1-propene 3,3-DIACETOXY-1-PROPENE 1,1-DIACETOXY-2-PROPENE Acrolein diacetyl acetal 2-PROPENYLIDENE DIACETATE Acrolein hydrate diacetate 2-PROPENE-1,1-DIOL DIACETATE 1-acetyloxyprop-2-enyl acetate 1-acetyloxyprop-2-enyl ethanoate acetic acid 1-acetoxyallyl ester 2-Propene-1,1-diol,1,1-diacetate cetic acid 1-acetoxy-allyl ester 1-(Acetyloxy)-2-propenyl acetate Acrolein, monohydrate, diacetate 2-Propenal, monohydrate, diacetate
[EINECS(EC#)] 212-789-0
[Molecular Formula] C7H10O4
[MDL Number] MFCD00008708
[Molecular Weight] 158.15
[MOL File] 869-29-4.mol

Chemical Properties	Back Directory
[Melting point ] -37.6°C
[Boiling point ] 180°C (estimate)
[density ] 1.0760
[refractive index ] 1.4193 (estimate)
[CAS DataBase Reference] 869-29-4(CAS DataBase Reference)
[EPA Substance Registry System] 2-Propene-1,1-diol diacetate (869-29-4)

Safety Data	Back Directory
[Risk Statements ] R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ] S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice . S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
[RIDADR ] 2810
[HazardClass ] 6.1(a)
[PackingGroup ] II

Hazard Information	Back Directory
[Synthesis Reference(s)] The Journal of Organic Chemistry, 48, p. 1765, 1983 DOI: 10.1021/jo00158a036
[Purification Methods] Check the NMR spectrum. If it is not satisfactory, then add Ac2O and a drop of conc H2SO4 and heat at 50o for 10minutes. Then add anhydrous NaOAc (ca 3g/ 100g of liquid) and fractionate. Note that it forms an azeotrope with H2O, so do not add H2O at any time. It is a highly flammable and TOXIC liquid; keep away from the skin. [Smith et al. J Am Chem Soc 73 5282 1951, Beilstein 2 H 154, 2 I 72, 2 III 356, 2 IV 291.]

Spectrum Detail	Back Directory
[Spectrum Detail] ALLYLIDENE DIACETATE(869-29-4)MS ALLYLIDENE DIACETATE(869-29-4)¹³CNMR ALLYLIDENE DIACETATE(869-29-4)IR1

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