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90-11-9

90-11-9 Structure

90-11-9 Structure
IdentificationMore
[Name]

1-Bromonaphthalene
[CAS]

90-11-9
[Synonyms]

1-BROMONAPHTHALENE
A-BROMONAPHTHALENE
ALPHA-BROMONAPHTHALENE
ALPHA-MONOBROMONAPHTHALENE
ALPHA-NAPHTHYL BROMIDE
1-bromo-naphthalen
1-Naphthyl bromide
1-naphthylbromide
-Bromonaphthalene
I-Bromnaphthalin
Naphthalene,1-bromo-
α-bromonaphthalene
1-BROMO NAPTHALENE
1-Bromonaphtalene
1-Bromonaphthalene solution
1-BROMONAPHTHALENE STABILIZED
1-BROMONAPHTHALENE SOLUTION, IN PARAFFIN OIL
1-BromonaphthaleneForSynthesis
1-Bromonaphthalene96%
1-Bromonaphthalene,~99%
[EINECS(EC#)]

201-965-2
[Molecular Formula]

C10H7Br
[MDL Number]

MFCD00003868
[Molecular Weight]

207.07
[MOL File]

90-11-9.mol
Chemical PropertiesBack Directory
[Appearance]

clear yellow to yellow-brown liquid
[Melting point ]

−2-−1 °C(lit.)
[mp ]

−2-−1 °C(lit.)
[Boiling point ]

133-134 °C10 mm Hg(lit.)
[bp ]

133-134 °C10 mm Hg(lit.)
[density ]

1.48 g/mL at 20 °C(lit.)
[vapor pressure ]

0.013 hPa (20 °C)
[refractive index ]

n20/D 1.6570(lit.)
[Fp ]

>230 °F
[storage temp. ]

Store below +30°C.
[solubility ]

H2O: slightly soluble
[form ]

Liquid
[color ]

slightly yellow to deep brownish-yellow
[Water Solubility ]

slightly soluble
[Merck ]

14,1425
[Detection Methods]

GC
[BRN ]

1906414
[InChIKey]

DLKQHBOKULLWDQ-UHFFFAOYSA-N
[CAS DataBase Reference]

90-11-9(CAS DataBase Reference)
[NIST Chemistry Reference]

Naphthalene, 1-bromo-(90-11-9)
[EPA Substance Registry System]

90-11-9(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

Xn,Xi
[Risk Statements ]

R22:Harmful if swallowed.
R36:Irritating to the eyes.
R36/37/38:Irritating to eyes, respiratory system and skin .
R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[RIDADR ]

2810
[WGK Germany ]

3
[RTECS ]

QJ1545000
[F ]

8
[TSCA ]

Yes
[HazardClass ]

6.1(b)
[PackingGroup ]

III
[HS Code ]

29036990
[Toxicity]

LD50 orally in Rabbit: 810 mg/kg
Raw materials And Preparation ProductsBack Directory
【Raw materials】

Government regulation-->Carbon tetrachloride-->1-Chloronaphthalene
【Preparation Products】

N,N'-Bis- (1-naphthalenyl)-N,N'-bis-phenyl-(1,1'-biphenyl)-4,4'-diamine-->1-Naphthoic acid-->1-NAPHTHALENETHIOL-->1-Naphthylboronic acid-->1-Cyanonaphthalene-->1'-Acetonaphthone-->4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione-->1-(4-Bromophenyl)-naphthlene-->(4R,5R)-(-)-2,2-DIMETHYL-ALPHA,ALPHA,ALPHA',ALPHA'-TETRA(1-NAPHTHYL)-1,3-DIOXOLANE-4,5-DIMETHANOL-->1-Bromo-4-chloronaphthalene-->1-(2-CHLOROETHYL)NAPHTHALENE-->Benzenamine, 4-(1-naphthalenyl)--->1-NAPHTHYLMAGNESIUM BROMIDE
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

alpha-Bromonaphthalene(90-11-9).msds
Hazard InformationBack Directory
[Chemical Properties]

clear yellow to yellow-brown liquid
[Synthesis Reference(s)]

Organic Syntheses, Coll. Vol. 1, p. 121, 1941
Tetrahedron, 64, p. 4999, 2008 DOI: 10.1016/j.tet.2008.03.085
[Purification Methods]

Purify 1-bromonaphthalene by passage through activated alumina, and three vacuum distillations. [Beilstein 5 H 547, 5 IV 1665.]
Spectrum DetailBack Directory
[Spectrum Detail]

1-Bromonaphthalene(90-11-9) 1H NMR
1-Bromonaphthalene(90-11-9) Raman
1-Bromonaphthalene(90-11-9) MS
1-Bromonaphthalene(90-11-9) IR2
1-Bromonaphthalene(90-11-9) IR1
1-Bromonaphthalene(90-11-9) 13C NMR
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

1-Bromonaphthalene, 96%(90-11-9)
[Alfa Aesar]

1-Bromonaphthalene, 97%(90-11-9)
[Sigma Aldrich]

90-11-9(sigmaaldrich)
[TCI AMERICA]

1-Bromonaphthalene,>95.0%(GC)(90-11-9)
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