ChemicalBook--->CAS DataBase List--->92-85-3

92-85-3

92-85-3 Structure

92-85-3 Structure
IdentificationMore
[Name]

Thianthrene
[CAS]

92-85-3
[Synonyms]

AKOS 90207
DI-O-PHENYLENE DISULFIDE
DIPHENYLENE DISULFIDE
THIANTHRENE
9,10-Dithiaanthracene
dibenzo-1,4-dithiin
Thiaanthrene
Thianthren
THIANTHRENE, 99+%
diphylene disulfide
Dibenzodithiodioxane
[EINECS(EC#)]

202-197-0
[Molecular Formula]

C12H8S2
[MDL Number]

MFCD00005065
[Molecular Weight]

216.32
[MOL File]

92-85-3.mol
Chemical PropertiesBack Directory
[Melting point ]

151-155 °C (lit.)
[Boiling point ]

364-366 °C (lit.)
[density ]

1.4420
[refractive index ]

1.6210 (estimate)
[storage temp. ]

Sealed in dry,Room Temperature
[solubility ]

DMF: soluble
[form ]

powder to crystal
[color ]

White to Light yellow
[BRN ]

83046
[CAS DataBase Reference]

92-85-3(CAS DataBase Reference)
[NIST Chemistry Reference]

Thianthrene(92-85-3)
[EPA Substance Registry System]

92-85-3(EPA Substance)
Safety DataBack Directory
[Safety Statements ]

24/25
[WGK Germany ]

3
[HS Code ]

29349990
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

Thianthrene(92-85-3).msds
Hazard InformationBack Directory
[Chemical Properties]

White to off-white solid
[Uses]

Thianthrene has been used to study aqueous solubilities of several solid nitrogen-, sulfur- and oxygen-containing heterocyclic derivatives of anthracene, phenanthrene and fluorene. It has been used in determination of partition coefficients of several sulfur-containing aromatics in 1-hexyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide and supercritical carbon dioxide.
[Definition]

ChEBI: The organosulfur heterocyclic compound that is the parent compound of the thianthrenes, a tricyclic structure comprising two benzene rings fused to the b and e sides of 1,4-dithin.
[Synthesis Reference(s)]

The Journal of Organic Chemistry, 31, p. 4071, 1966 DOI: 10.1021/jo01350a045
[General Description]

Thianthrene undergoes liquid phase tert-butylation in the presence of large pore zeolites and mesoporous aluminosilicates catalyst to yield tert-butyl derivatives. Thianthrene on oxidation in the presence of hydrogen peroxide and ligninase as catalyst from Phanerochaete chrysosporium yields thianthrene monosulfoxide.
[storage]

Store at -20°C
[Purification Methods]

thianthrene from Me2CO (charcoal), AcOH or EtOH. It sublimes in a vacuum. [Beilstein 19 H 45, 19 I 619, 19 II 34, 19 III/IV 347, 19/2 V 49.]
Spectrum DetailBack Directory
[Spectrum Detail]

Thianthrene(92-85-3)MS
Thianthrene(92-85-3)1HNMR
Thianthrene(92-85-3)13CNMR
Thianthrene(92-85-3)IR1
Thianthrene(92-85-3)IR2
Thianthrene(92-85-3)Raman
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

92-85-3(sigmaaldrich)
[TCI AMERICA]

Thianthrene,>98.0%(GC)(92-85-3)
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