(R)-1-(2,4-Dichlorophenyl)ethanamine

(R)-1-(2,4-Dichlorophenyl)ethanamine Struktur
133773-29-2
CAS-Nr.
133773-29-2
Englisch Name:
(R)-1-(2,4-Dichlorophenyl)ethanamine
Synonyma:
EOS-60919;(R)-1-(2,4-chlorophenyl)ethanaMine;(R)-1-(2,4-DICHLOROPHENYL)ETHANAMINE;(1R)-1-(2,4-dichlorophenyl)ethylamine;(R)-1-(2,4-dichlorophenyl)ethan-1-amine;(1R)-1-(2,4-DICHLOROPHENYL)ETHAN-1-AMINE;Benzenemethanamine, 2,4-dichloro-α-methyl-, (αR)-;(1R)-1-(2,4-Dichlorophenyl)ethanamine Hydrochloride
CBNumber:
CB0168881
Summenformel:
C8H9Cl2N
Molgewicht:
190.07
MOL-Datei:
Mol file

(R)-1-(2,4-Dichlorophenyl)ethanamine Eigenschaften

Siedepunkt:
256.4±25.0 °C(Predicted)
Dichte
1.262±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
8.28±0.10(Predicted)
Aggregatzustand
liquid
Farbe
Colourless
Sicherheit
  • Risiko- und Sicherheitserklärung
  • Gefahreninformationscode (GHS)
HS Code  2921490090
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H302 Gesundheitsschädlich bei Verschlucken. Akute Toxizität oral Kategorie 4 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P270, P301+P312, P330, P501
H315 Verursacht Hautreizungen. Hautreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P302+P352, P321,P332+P313, P362
H319 Verursacht schwere Augenreizung. Schwere Augenreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P305+P351+P338,P337+P313P
H335 Kann die Atemwege reizen. Spezifische Zielorgan-Toxizität (einmalige Exposition) Kategorie 3 (Atemwegsreizung) Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" />
Sicherheit
P261 Einatmen von Staub vermeiden.
P305+P351+P338 BEI KONTAKT MIT DEN AUGEN: Einige Minuten lang behutsam mit Wasser spülen. Eventuell vorhandene Kontaktlinsen nach Möglichkeit entfernen. Weiter spülen.

(R)-1-(2,4-Dichlorophenyl)ethanamine Chemische Eigenschaften,Einsatz,Produktion Methoden

Synthese

(5)-Mandelic acid (40.2 g, 264.5 mmol) was added to a solution of 3:2 isopropyl alcohol (/PrOH) and ethanol (EtOH) (500 mL) at room temperature, and the suspension was heated at 60 °C until a clear solution formed. Racemic 2,4-dichloro-a-methyl benzylamine (50 g, 264.5 mmol) was added to the hot solution, which was then cooled to 30 °C over 2 h and stirred at this temperature for 24 h. The colorless crystals were collected by filtration and washed with acetone (70 mL). The resulting salt was suspended in 3:2 /PrOH/EtOH (400 mL) at room temperature and the mixture was heated at 60 °C to give a clear solution. The solution was then cooled to room temperature and stirred for 24 hours. The colorless crystals were filtered off, and washed with acetone (40 mL) to give the desired salt. A portion of the salt (12.0 g) in dichloromethane (CH2C12) (100 mL) was added to aqueous 4 N sodium hydroxide solution (30 mL). The reaction mixture was stirred for 1 h at room temperature, and extracted with dichloromethane (2 χ 100 mL), dried with anhydrous sodium sulfate (Na2S04), filtered, and concentrated in vacuo to afford (R)-1-(2,4-Dichlorophenyl)ethanamine as a colorless liquid (7.5 g, 39.5 mmol, 40%).
(R)-1-(2,4-DICHLOROPHENYL)ETHANAMINE

(R)-1-(2,4-Dichlorophenyl)ethanamine Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


(R)-1-(2,4-Dichlorophenyl)ethanamine Anbieter Lieferant Produzent Hersteller Vertrieb Händler.

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  • (R)-1-(2,4-DICHLOROPHENYL)ETHANAMINE
  • (1R)-1-(2,4-DICHLOROPHENYL)ETHAN-1-AMINE
  • (R)-1-(2,4-chlorophenyl)ethanaMine
  • (R)-1-(2,4-dichlorophenyl)ethan-1-amine
  • (1R)-1-(2,4-Dichlorophenyl)ethanamine Hydrochloride
  • (1R)-1-(2,4-dichlorophenyl)ethylamine
  • Benzenemethanamine, 2,4-dichloro-α-methyl-, (αR)-
  • EOS-60919
  • 133773-29-2
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