Prednisone Impurity 13

Prednisone Impurity 13 Struktur
91160-89-3
CAS-Nr.
91160-89-3
Englisch Name:
Prednisone Impurity 13
Synonyma:
BNKY015-BD02;Prednisone Impurity 5;Prednisone Impurity 13;Budesonide Impurity 53;9α-bromo-11β,16α,17α,21-tetrahydroxypregnane-1,4-diene-3,20-dione-21-acetate;9α-bromo-11β,16α,17α,21-tetrahydroxypregnane-1,4-diene-3,20-dione-21-acetate;(11β,16α)-21-(Acetyloxy)-9-bromo-11,16,17-trihydroxy-pregna-1,4-diene-3,20-dione;Pregna-1,4-diene-3,20-dione, 21-(acetyloxy)-9-bromo-11,16,17-trihydroxy-, (11β,16α)-;((8S,9R,10S,11S,13S,14S,16R,17S)-9-bromo-11,16,17-trihydroxy-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxoethyl acetate;2-((8S,9R,10S,11S,13S,14S,16R,17S)-9-bromo-11,16,17-trihydroxy-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxoethyl acetate
CBNumber:
CB44844383
Summenformel:
C23H29BrO7
Molgewicht:
497.38
MOL-Datei:
91160-89-3.mol

Prednisone Impurity 13 Eigenschaften

Siedepunkt:
636.3±55.0 °C(Predicted)
Dichte
1.53±0.1 g/cm3(Predicted)
pka
11.57±0.70(Predicted)

Sicherheit

Prednisone Impurity 13 Chemische Eigenschaften,Einsatz,Produktion Methoden

Synthese

50.5 g of 2-((8S,10S,13S,14S,16R,17S)-16,17-dihydroxy-10,13-dimethyl-3-oxo-6,7,8,10,12,13,14,15,16,17-decahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxoethyl acetate was dissolved in 1500 ml of acetone, 70 ml of 5% perchloric acid was added, the temperature was lowered to 0°C with stirring, and 45 g of N-bromosuccinimide was added and stirred After the reaction was completed, 50 ml of 20% sodium sulfite aqueous solution was added, the acetone was concentrated, the water was separated, filtered, and dried to obtain 62 g of Prednisone Impurity 13 (9α-bromo-11β,16α,17α,21-tetrahydroxypregnane-1,4-diene-3,20-dione-21-acetate).
Prednisone Impurity 13

Prednisone Impurity 13 Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


Prednisone Impurity 13 Anbieter Lieferant Produzent Hersteller Vertrieb Händler.

Global( 17)Lieferanten
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BIONNA MEDICINE CO.,LTD
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Hubei Yangxin Medical Technology Co., Ltd. 15374522761
3003392093@qq.com China 7851 55
Hubei Moco Chemical Co., Ltd. 18627756402
3001051413@qq.com China 10014 58
Jinan blalong chemical co. LTD 2710913286@.com
1513643261@qq.com China 14253 58
Bono Kangyuan (Beijing) Pharmaceutical Technology Co., Ltd 010-56380788-8515 16619769925
wch013@bionna.cn China 53 58
Wuxi Helen Biotechnology Co., Ltd., 0510-85629785 18013409632
sales@reading-chemicals.com China 14092 58
Meng Cheng Technology (Shanghai) Co., LTD 400-820-6829
sales@mitachieve.com China 8864 58

  • Prednisone Impurity 13
  • 9α-bromo-11β,16α,17α,21-tetrahydroxypregnane-1,4-diene-3,20-dione-21-acetate
  • BNKY015-BD02
  • (11β,16α)-21-(Acetyloxy)-9-bromo-11,16,17-trihydroxy-pregna-1,4-diene-3,20-dione
  • Pregna-1,4-diene-3,20-dione, 21-(acetyloxy)-9-bromo-11,16,17-trihydroxy-, (11β,16α)-
  • 9α-bromo-11β,16α,17α,21-tetrahydroxypregnane-1,4-diene-3,20-dione-21-acetate
  • Prednisone Impurity 5
  • Budesonide Impurity 53
  • ((8S,9R,10S,11S,13S,14S,16R,17S)-9-bromo-11,16,17-trihydroxy-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxoethyl acetate
  • 2-((8S,9R,10S,11S,13S,14S,16R,17S)-9-bromo-11,16,17-trihydroxy-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-17-yl)-2-oxoethyl acetate
  • 91160-89-3
  • C23H29BrO7
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