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CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER

CAS No.
161117-88-0
Chemical Name:
CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER
Synonyms
tert-butyl 5-nitropyridin-2-ylcarbaMate;tert-butyl N-(5-nitro-2-pyridyl)carbamate;tert-butyl N-(5-nitropyridin-2-yl)carbamate;tert-butyl N-(5-nitro-2-pyridyl)carbamate - [B83341];N-(5-nitro-2-pyridinyl)carbamic acid tert-butyl ester;CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER;Carbamic acid, N-(5-nitro-2-pyridinyl)-, 1,1-dimethylethyl ester
CBNumber:
CB02468075
Molecular Formula:
C10H13N3O4
Molecular Weight:
239.23
MDL Number:
MFCD11977408
MOL File:
161117-88-0.mol
MSDS File:
SDS
Last updated:2025-07-24 18:13:45

CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER Properties

Boiling point 325.2±27.0 °C(Predicted)
Density 1.303±0.06 g/cm3(Predicted)
storage temp. Inert atmosphere,Room Temperature
pka 11.35±0.70(Predicted)
Appearance Light yellow to yellow Solid

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H302-H317-H319
Precautionary statements  P280-P305+P351+P338
Hazard Codes  Xn
Risk Statements  22-36-43
Safety Statements  26-36/37

CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER price More Price(21)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TRC B700748 tert-Butyl(5-Nitropyridin-2-yl)carbamate 161117-88-0 500mg $155 2021-12-16 Buy
Matrix Scientific 150581 tert-Butyl (5-nitropyridin-2-yl)carbamate 95% 161117-88-0 5g $1172 2021-12-16 Buy
Matrix Scientific 150581 tert-Butyl (5-nitropyridin-2-yl)carbamate 95% 161117-88-0 1g $378 2021-12-16 Buy
Biosynth Carbosynth FB54521 tert-Butyl 5-nitropyridin-2-ylcarbamate 161117-88-0 1g $401.8 2021-12-16 Buy
American Custom Chemicals Corporation CHM0394226 TERT-BUTYL-(5-NITROPYRIDIN-2-YL)CARBAMATE 95.00% 161117-88-0 5MG $499.5 2021-12-16 Buy
Product number Packaging Price Buy
B700748 500mg $155 Buy
150581 5g $1172 Buy
150581 1g $378 Buy
FB54521 1g $401.8 Buy
CHM0394226 5MG $499.5 Buy

CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER Chemical Properties,Uses,Production

Synthesis

2-Amino-5-nitropyridine

4214-76-0

Di-tert-butyl dicarbonate

24424-99-5

CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER

161117-88-0

5-Nitropyridin-2-amine (1 eq.), di-tert-butyl dicarbonate (1.2 eq.) and 4-dimethylaminopyridine (0.2 eq.) were added to a reaction vial under nitrogen protection. Dichloromethane was added as solvent at room temperature and the reaction mixture was stirred overnight. Upon completion of the reaction, ethyl acetate was added to the crude product, the precipitate was collected by filtration and washed with ethyl acetate to afford the target product (5-nitropyridin-2-yl)carbamic acid tert-butyl ester. It was analyzed by HPLC-MS (Method A): retention time (Rt) = 2.88 min, m/z of [M + H]+: 240. 80% yield.

References

[1] Patent: WO2016/120808, 2016, A1. Location in patent: Page/Page column 103; 104
[2] Patent: EP2314593, 2016, B1. Location in patent: Paragraph 0132
[3] Patent: WO2015/131080, 2015, A1. Location in patent: Paragraph 001167; 001168
[4] Patent: US2010/249099, 2010, A1. Location in patent: Page/Page column 96-97
[5] Patent: US2011/9405, 2011, A1. Location in patent: Page/Page column 54

CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER Preparation Products And Raw materials

CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER Suppliers

Global( 36)Suppliers
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Hong Kong Tiansheng New Material Trading Co., Ltd
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ShangHai KenEn Chemical Technology Co., Ltd. 13120367189 mychess007@163.com China 1994 55
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View Lastest Price from CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
tert-Butyl (5-nitropyridin-2-yl)carbamate pictures 2022-02-25 tert-Butyl (5-nitropyridin-2-yl)carbamate
161117-88-0
US $11.00 / KG 1KG 99% 50kg Hong Kong Tiansheng New Material Trading Co., Ltd
tert-Butyl (5-nitropyridin-2-yl)carbamate pictures 2022-02-25 tert-Butyl (5-nitropyridin-2-yl)carbamate
161117-88-0
US $11.00 / KG 1KG 98% 100KG Hong Kong Tiansheng New Material Trading Co., Ltd
tert-Butyl (5-nitropyridin-2-yl)carbamate pictures 2022-02-25 tert-Butyl (5-nitropyridin-2-yl)carbamate
161117-88-0
US $11.00 / KG 1KG 98% 100KG Hong Kong Tiansheng New Material Trading Co., Ltd

CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER Spectrum

tert-butyl 5-nitropyridin-2-ylcarbaMate CARBAMIC ACID, (5-NITRO-2-PYRIDINYL)-, 1,1-DIMETHYLETHYL ESTER N-(5-nitro-2-pyridinyl)carbamic acid tert-butyl ester Carbamic acid, N-(5-nitro-2-pyridinyl)-, 1,1-dimethylethyl ester tert-butyl N-(5-nitro-2-pyridyl)carbamate tert-butyl N-(5-nitropyridin-2-yl)carbamate tert-butyl N-(5-nitro-2-pyridyl)carbamate - [B83341] 161117-88-0