Ethyl 2,5-Dioxopyrrole-1-carboxylate
- CAS No.
- 55750-49-7
- Chemical Name:
- Ethyl 2,5-Dioxopyrrole-1-carboxylate
- Synonyms
- NSC 266054;N-Carbethoxymaleimide;N-Ethoxycarbonylmaleimide;N-Ethyoxycarbonyl MaleiMide;Ethyl 2,5-Dioxopyrrole-1-carboxylate;ethyl 2,5-dioxo-2H-pyrrole-1(5H)-carboxylate;Ethyl 2,5-dioxo-2,5-dihydro-1H-pyrrole-1-carboxylate;1H-Pyrrole-1-carboxylic acid, 2,5-dihydro-2,5-dioxo-, ethyl ester
- CBNumber:
- CB12520705
- Molecular Formula:
- C7H7NO4
- Molecular Weight:
- 169.13
- MDL Number:
- MFCD16619570
- MOL File:
- 55750-49-7.mol
Ethyl 2,5-Dioxopyrrole-1-carboxylate price More Price(13)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Usbiological | 448986 | Ethyl 2,5-dioxopyrrole-1-carboxylate | 55750-49-7 | 100mg | $305 | 2021-12-16 | Buy |
| Apolloscientific | OR953252 | Ethyl2,5-dioxopyrrole-1-carboxylate 95% | 55750-49-7 | 5g | $395 | 2021-12-16 | Buy |
| Apolloscientific | OR953252 | Ethyl2,5-dioxopyrrole-1-carboxylate 95% | 55750-49-7 | 1g | $115 | 2021-12-16 | Buy |
| Ambeed | A191928 | Ethyl2,5-dioxo-2,5-dihydro-1H-pyrrole-1-carboxylate 97% | 55750-49-7 | 5g | $130 | 2021-12-16 | Buy |
| Chemenu | CM197916 | ethyl2,5-dioxo-2,5-dihydro-1H-pyrrole-1-carboxylate 97% | 55750-49-7 | 5g | $184 | 2021-12-16 | Buy |
Ethyl 2,5-Dioxopyrrole-1-carboxylate Chemical Properties,Uses,Production
Synthesis
541-59-3
541-41-3
55750-49-7
1) Synthesis of ethyl 2,5-dioxo-2,5-dihydro-1H-pyrrole-1-carboxylate: 9.7 g (0.1 mol) of maleimide was dissolved in a mixed solution of 50 ml of ethyl acetate and 1.1 ml of N-methylmorpholine at 5 °C. Slowly 1.1 ml of ethyl chloroformate was added dropwise to the above solution. The reaction mixture was stirred at the same temperature for 30 minutes. After completion of the reaction, insoluble impurities were removed by filtration. The filtrate was washed with 50 ml of water and the organic phase was separated and dried with anhydrous magnesium sulfate. The dried organic phase was concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography (Merck Geduran silica gel, 40-63 μm) with dichloromethane/ethyl acetate (66/34, v/v) as eluent. Finally, 16.9 g of pure product was obtained in 50% yield. Mass spectrometry results: m/z = 170.1 (ES+), theoretical molecular weight M = 169.
References
[1] Organic Letters, 2015, vol. 17, # 23, p. 5846 - 5849
[2] Chemical Communications, 2014, vol. 50, # 7, p. 859 - 861
[3] Patent: US2010/297025, 2010, A1
[4] Patent: US9273304, 2016, B2. Location in patent: Page/Page column 16
Ethyl 2,5-Dioxopyrrole-1-carboxylate Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29855 | 58 |
| SHANDONG ZHI SHANG CHEMICAL CO.LTD | +86 18953170293 | sales@sdzschem.com | China | 2930 | 58 |
| Accela ChemBio Inc. | +1-858-6993322 | info@accelachem.com | United States | 21193 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| Hubei Ipure Biology Co., Ltd | +8613367258412 | ada@ipurechemical.com | China | 10244 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | sales@tnjchem.com | China | 34563 | 58 |
| Win-Win chemical CO., Limited | +86-0086-577-64498589 +86-15355981851 | sales@win-winchemical.com | China | 14459 | 58 |
| Nextpeptide Inc | +86-0571-81612335 +8613336028439 | sales@nextpeptide.com | China | 19908 | 58 |
| Labnetwork lnc. | +86-27-50766799 +8618062016861 | contact@labnetwork.com | China | 19987 | 58 |
| Wuhan Konberd Biotech Co., Ltd | +undefined18986093962 | admin@konberdbio.com | China | 1379 | 58 |
View Lastest Price from Ethyl 2,5-Dioxopyrrole-1-carboxylate manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2019-09-02 | Ethyl 2,5-Dioxopyrrole-1-carboxylate
55750-49-7
|
US $1.00 / KG | 1KG | ≥98% | 200KG | Career Henan Chemical Co |
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- Ethyl 2,5-Dioxopyrrole-1-carboxylate
55750-49-7
- US $1.00 / KG
- ≥98%
- Career Henan Chemical Co