Methyl2-Amino-4-Iodobenzoate
- CAS No.
- 144550-76-5
- Chemical Name:
- Methyl2-Amino-4-Iodobenzoate
- Synonyms
- Methyl2-Amino-4-Iodobenzoate;Benzoic acid, 2-amino-4-iodo-, methyl ester
- CBNumber:
- CB41028131
- Molecular Formula:
- C8H8INO2
- Molecular Weight:
- 277.06
- MDL Number:
- MFCD13182440
- MOL File:
- 144550-76-5.mol
- MSDS File:
- SDS
Methyl2-Amino-4-Iodobenzoate price More Price(36)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS47430 | Methyl 2-amino-4-iodobenzoate 97% | 144550-76-5 | 1g | $75 | 2026-06-04 | Buy |
| Activate Scientific | AS47430 | Methyl 2-amino-4-iodobenzoate 97% | 144550-76-5 | 5g | $163 | 2026-06-04 | Buy |
| Synthonix | M36798 | Methyl 2-amino-4-iodobenzoate | 144550-76-5 | 250mg | $44 | 2026-05-06 | Buy |
| Synthonix | M36798 | Methyl 2-amino-4-iodobenzoate | 144550-76-5 | 1g | $50 | 2026-05-06 | Buy |
| Synthonix | M36798 | Methyl 2-amino-4-iodobenzoate | 144550-76-5 | 5g | $150 | 2026-05-06 | Buy |
Methyl2-Amino-4-Iodobenzoate Chemical Properties, Uses, Production
Synthesis
67-56-1
117324-10-4
144550-76-5
General procedure for the synthesis of methyl 2-amino-4-iodobenzoate from methanol and 2-acetamido-4-iodobenzoic acid (CAS:117324-10-4): 16.1 g of 2-acetamido-4-iodobenzoic acid (melting point 233°C-235°C; synthesized according to U.S. Patent 4,762,838) was dissolved in 325 ml of anhydrous methanol, cooled to 0°C and passed through a dry hydrogen chloride gas to saturation. The reaction mixture was heated to reflux for 15 hours, cooled to room temperature and again passed through dry HCl gas to saturation, followed by standing at room temperature for 24 hours. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure and the residue was dissolved in dichloromethane. The organic phase was washed to neutrality with saturated aqueous sodium bicarbonate to remove unreacted acid. The organic phase was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 13.8 g of methyl 2-amino-4-iodobenzoate with a melting point of 63°C-67°C.
References
[1] Patent: WO2006/41773, 2006, A2. Location in patent: Page/Page column 303-304
[2] Patent: US2017/121294, 2017, A1. Location in patent: Paragraph 0058
Methyl2-Amino-4-Iodobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
Methyl2-Amino-4-Iodobenzoate Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Carbott PharmTech Inc. | 0535-6385396 | info@carbottpharm.com | China | 995 | 56 |
| Shanghai Hanhong Scientific Co.,Ltd. | 021-54306202 13764082696 | info@hanhongsci.com | China | 42917 | 64 |
| SynAsst Chemical. | 021-60343070 | China | 12731 | 55 | |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Yantai ShengKailun Chemical Technology Co., Ltd. | 13356901049 | 3119594100@qq.com | China | 7964 | 55 |
| Aikon International Limited | 025-66061636 19370895928 | qqyang@aikonchem.com | China | 15810 | 58 |
| Suzhou Nuoouman Biological Technology Co., Ltd. | 15026866316 | 180642609@qq.com | China | 4965 | 58 |
| Suzhou Xiya Pharmaceutical Co., Ltd. | 0512-87819718 18912655635 | 2587879032@qq.com | China | 1273 | 58 |
| Cool Pharm, Ltd | 021-58581007 18019463053 | sales@coolpharm.com | China | 9999 | 58 |
| Shanghai Yanze Chemical Co., Ltd. | 15345144255 19901447308 | 260924549@qq.com | China | 9989 | 58 |
