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4-BroMo-9H-carbazole

CAS No.
3652-89-9
Chemical Name:
4-BroMo-9H-carbazole
Synonyms
4-broMocarbazole;Carb;9H-Carbazole, 4-broMo-;Carbazole, 4-bromo-;4-bromo-1H-carbazole;4-Bromocarbazole >4-BroMo-9H-carbazole;4-BroMo-9H-carbazole (4BC);1-CYCLOPROPYL-2,6-PIPERAZINEDIONE;4-BroMo-9H-carbazole ISO 9001:2015 REACH
CBNumber:
CB52642696
Molecular Formula:
C12H8BrN
Molecular Weight:
246.1
MDL Number:
MFCD18450175
MOL File:
3652-89-9.mol
MSDS File:
SDS
Last updated:2023-12-22 17:53:22

4-BroMo-9H-carbazole Properties

Melting point 104-105℃
Boiling point 409.2±18.0 °C(Predicted)
Density 1.617±0.06 g/cm3 (20 ºC 760 Torr)
storage temp. Sealed in dry,Room Temperature
form powder to crystal
pka 16.04±0.30(Predicted)
color White to Light yellow
InChIKey CBJHFGQCHKNNJY-UHFFFAOYSA-N

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319
Precautionary statements  P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313
HS Code  2933998090

4-BroMo-9H-carbazole price More Price(24)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical B4752 4-Bromocarbazole >98.0%(GC) 3652-89-9 1g $106 2024-03-01 Buy
TCI Chemical B4752 4-Bromocarbazole >98.0%(GC) 3652-89-9 200mg $37 2024-03-01 Buy
TRC B678898 4-Bromo-9H-carbazole 3652-89-9 25mg $75 2021-12-16 Buy
SynQuest Laboratories 3H31-9-1B 4-Bromo-9H-carbazole 99% 3652-89-9 25g $568 2021-12-16 Buy
AK Scientific 6426AL 4-Bromo-9H-carbazole 3652-89-9 250mg $57 2021-12-16 Buy
Product number Packaging Price Buy
B4752 1g $106 Buy
B4752 200mg $37 Buy
B678898 25mg $75 Buy
3H31-9-1B 25g $568 Buy
6426AL 250mg $57 Buy

4-BroMo-9H-carbazole Chemical Properties,Uses,Production

Chemical Properties

White powder.

Uses

4-BroMo-9H-carbazole is a useful research chemical. 4-BroMo-9H-carbazole is a bromide-substitution of carbazole. The carbazole ring system is essentially planar (r.m.s. deviation of 0.024A for the non-H atoms). It is a photoelectric material intermediate and be used to synthesize OLED materials.    

Hazard

H315 (100%): Causes skin irritation [Warning Skin corrosion/irritation]
H319 (100%): Causes serious eye irritation [Warning Serious eye damage/eye irritation]

Synthesis

Under nitrogen protection,Add 357.6g m-dibromobenzene (99%, 1.5mol) into a 500mL reaction flask,26.1g o-bromoaniline (99%, 0.15mol),0.084g palladium(II) acetate (99%, 0.375mmol),0.18g 2-dicyclohexylphosphine-2,4,6-triisopropylbiphenyl (99%, 0.375mmol),58.2g sodium tert-butoxide (99%, 0.6mol),After feeding,Warm up to 130°C,Stirring speed 600rpm,Incubate for 24hr,After the reaction,Vacuum distillation to recover unreacted m-dibromobenzene,Add water and ethyl acetate to extract the residue,The organic layer was desolvated to obtain the crude product which was crystallized in ethanol to obtain 34.3 g of 4-BroMo-9H-carbazole.The content is 99.6% and the yield is 92.5%.3652-89-9-b.png

108-36-1
615-36-1
3652-89-9
Synthesis of 4-BroMo-9H-carbazole from 1,3-Dibromobenzene and 2-Bromoaniline

4-BroMo-9H-carbazole Preparation Products And Raw materials

Global( 226)Suppliers
Supplier Tel Email Country ProdList Advantage
Springchem New Material Technology Co.,Limited
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Henan Fengda Chemical Co., Ltd
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Capot Chemical Co.,Ltd.
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Henan Tianfu Chemical Co.,Ltd.
+86-0371-55170693 +86-19937530512 info@tianfuchem.com China 21691 55
Nanjing ChemLin Chemical Industry Co., Ltd.
025-83697070 product@chemlin.com.cn CHINA 3012 60

View Lastest Price from 4-BroMo-9H-carbazole manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
4-Bromo-9H-carbazole pictures 2024-04-26 4-Bromo-9H-carbazole
3652-89-9
US $0.00-0.00 / kg 1kg 98%+ 1000kg per Month Shanghai Qyubiotech Co., Ltd.
4-bromo-1H-carbazole pictures 2024-03-28 4-bromo-1H-carbazole
3652-89-9
US $0.00 / kg 25kg 98%-99% Inquiry PNP Biotech Co. Ltd
4-BroMo-9H-carbazole pictures 2023-12-23 4-BroMo-9H-carbazole
3652-89-9
US $50.00-1.00 / KG 1KG 99% g-kg-tons, free sample is available Henan Fengda Chemical Co., Ltd

4-BroMo-9H-carbazole Spectrum

4-BroMo-9H-carbazole 4-BroMo-9H-carbazole (4BC) 1-CYCLOPROPYL-2,6-PIPERAZINEDIONE Carbazole, 4-bromo- 4-Bromocarbazole > 4-bromo-1H-carbazole 4-BroMo-9H-carbazole ISO 9001:2015 REACH 4-broMocarbazole 9H-Carbazole, 4-broMo- Carb 1-[6-(4-fluoropyrazol-1-yl)pyridin-4-yl]ethanone 3652-89-9 OLED