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1,3-Benzodioxol-5-aMine, 6-iodo-

CAS No.
1000802-34-5
Chemical Name:
1,3-Benzodioxol-5-aMine, 6-iodo-
Synonyms
5-Amino-6-iodo-1,3-benzodioxole; 6-Iodo-1,3-benzodioxol-5-amine;1,3-Benzodioxol-5-aMine, 6-iodo-;6-iodobenzo[d][1,3]dioxol-5-aMine;6-Iodo-benzo[1,3]dioxol-5-ylamine
CBNumber:
CB92614518
Molecular Formula:
C7H6INO2
Molecular Weight:
263.03
MDL Number:
MFCD23728743
MOL File:
1000802-34-5.mol
MSDS File:
SDS
Last updated:2025-07-24 18:13:43
Product description Number Pack Size Price
6-Iodobenzo[d][1,3]dioxol-5-amine OR370010 250mg $387
6-IODOBENZO[D][1,3]DIOXOL-5-AMINE 95.00% HCH0368137 5MG $502.03
6-Iodobenzo[d][1,3]dioxol-5-amine 95+% AK127270 100mg $64
6-Iodobenzo[d][1,3]dioxol-5-amine 95+% A232480 250mg $113
6-Iodobenzo[d][1,3]dioxol-5-amine 95+% A232480 100mg $57
More product size

1,3-Benzodioxol-5-aMine, 6-iodo- Properties

storage temp. under inert gas (nitrogen or Argon) at 2–8 °C
Appearance Light yellow to brown Solid

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H302
Precautionary statements  P280-P305+P351+P338
HS Code  2932990090

1,3-Benzodioxol-5-aMine, 6-iodo- price More Price(15)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Apolloscientific OR370010 6-Iodobenzo[d][1,3]dioxol-5-amine 1000802-34-5 250mg $387 2021-12-16 Buy
American Custom Chemicals Corporation HCH0368137 6-IODOBENZO[D][1,3]DIOXOL-5-AMINE 95.00% 1000802-34-5 5MG $502.03 2021-12-16 Buy
Ark Pharm AK127270 6-Iodobenzo[d][1,3]dioxol-5-amine 95+% 1000802-34-5 100mg $64 2021-12-16 Buy
Ambeed A232480 6-Iodobenzo[d][1,3]dioxol-5-amine 95+% 1000802-34-5 250mg $113 2021-12-16 Buy
Ambeed A232480 6-Iodobenzo[d][1,3]dioxol-5-amine 95+% 1000802-34-5 100mg $57 2021-12-16 Buy
Product number Packaging Price Buy
OR370010 250mg $387 Buy
HCH0368137 5MG $502.03 Buy
AK127270 100mg $64 Buy
A232480 250mg $113 Buy
A232480 100mg $57 Buy

1,3-Benzodioxol-5-aMine, 6-iodo- Chemical Properties,Uses,Production

Synthesis

N-(6-iodobenzo[d][1,3]dioxol-5-yl)acetamide

1000802-33-4

1,3-Benzodioxol-5-aMine, 6-iodo-

1000802-34-5

N-(6-Iodobenzo[d][1,3]dioxol-5-yl)acetamide (200 mg, 0.656 mmol) was used as a raw material, which was dissolved with NaOH (1.31 g, 32.8 mmol) in a solvent mixture of ethanol (26 mL) and water (6 mL). The reaction mixture was heated to reflux under stirring and kept for 4 hours. Upon completion of the reaction, the mixture was cooled and the solvent was evaporated under reduced pressure. The residue was extracted by partitioning with dichloromethane (100 mL) and water (100 mL). The organic layer was separated and washed with distilled water (2 x 100 mL). The organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure to afford 6-iodobenzo[d][1,3]dioxol-5-amine (170 mg, 98% yield) as an orange solid. The product was analyzed by LC-MS showing [M+1]+ m/z 264; 1H NMR (DMSO-d6) δ 4.88 (s, 2H), 5.87 (s, 2H), 6.47 (s, 1H), 7.07 (s, 1H).

References

[1] Patent: US2008/234314, 2008, A1. Location in patent: Page/Page column 59
[2] Patent: US2010/184801, 2010, A1
[3] Patent: US2016/317508, 2016, A1. Location in patent: Paragraph 0181
[4] Patent: WO2008/47109, 2008, A1. Location in patent: Page/Page column 56
[5] Journal of Medicinal Chemistry, 2015, vol. 58, # 9, p. 3922 - 3943

1,3-Benzodioxol-5-aMine, 6-iodo- Preparation Products And Raw materials

Raw materials

Preparation Products

Global( 34)Suppliers
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ATK CHEMICAL COMPANY LIMITED
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View Lastest Price from 1,3-Benzodioxol-5-aMine, 6-iodo- manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
	6-Iodo-1,3-benzodioxol-5-amine pictures 2020-02-06 6-Iodo-1,3-benzodioxol-5-amine
1000802-34-5
US $1.00 / KG 1KG Min98% HPLC g/kg/ton Career Henan Chemical Co

1,3-Benzodioxol-5-aMine, 6-iodo- Spectrum

1,3-Benzodioxol-5-aMine, 6-iodo- 6-Iodo-benzo[1,3]dioxol-5-ylamine 6-iodobenzo[d][1,3]dioxol-5-aMine 6-Iodo-1,3-benzodioxol-5-amine 5-Amino-6-iodo-1,3-benzodioxole 1000802-34-5