テルル(IV)テトラブロミド
テルル(IV)テトラブロミド 物理性質
- 融点 :
- ~380 °C(lit.)
- 沸点 :
- 420 °C(lit.)
- 比重(密度) :
- 4.3 g/mL at 25 °C(lit.)
- 闪点 :
- 420°C
- 溶解性:
- reacts with H2O; soluble in ethyl ether
- 外見 :
- ビーズ
- 色:
- yellow-orange monoclinic
crystals, crystalline
- 水溶解度 :
- 水、エタノールと反応します。
- Sensitive :
- Moisture Sensitive
- Merck :
- 14,9125
- 暴露限界値:
- ACGIH: TWA 0.1 mg/m3
NIOSH: IDLH 25 mg/m3; TWA 0.1 mg/m3
- CAS データベース:
- 10031-27-3(CAS DataBase Reference)
- EPAの化学物質情報:
- Tellurium bromide (TeBr4), (T-4)- (10031-27-3)
安全性情報
- リスクと安全性に関する声明
- 危険有害性情報のコード(GHS)
絵表示(GHS) |
|
注意喚起語 |
危険 |
危険有害性情報 |
コード |
危険有害性情報 |
危険有害性クラス |
区分 |
注意喚起語 |
シンボル |
P コード |
H300 |
飲み込むと生命に危険 |
急性毒性、経口 |
1, 2 |
危険 |
|
P264, P270, P301+P310, P321, P330,P405, P501 |
H314 |
重篤な皮膚の薬傷?眼の損傷 |
皮膚腐食性/刺激性 |
1A, B, C |
危険 |
|
P260,P264, P280, P301+P330+ P331,P303+P361+P353, P363, P304+P340,P310, P321, P305+ P351+P338, P405,P501 |
H318 |
重篤な眼の損傷 |
眼に対する重篤な損傷性/眼刺激 性 |
1 |
危険 |
|
P280, P305+P351+P338, P310 |
|
注意書き |
P280 |
保護手袋/保護衣/保護眼鏡/保護面を着用するこ と。 |
P303+P361+P353 |
皮膚(または髪)に付着した場合:直ちに汚染された衣 類をすべて脱ぐこと/取り除くこと。皮膚を流水/シャワー で洗うこと。 |
P305+P351+P338 |
眼に入った場合:水で数分間注意深く洗うこと。次にコ ンタクトレンズを着用していて容易に外せる場合は外す こと。その後も洗浄を続けること。 |
P310 |
ただちに医師に連絡すること。 |
P405 |
施錠して保管すること。 |
|
テルル(IV)テトラブロミド 価格
もっと(2)
メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
富士フイルム和光純薬株式会社(wako)
|
W01SRM52-7000 |
臭化テルル(IV)
Tellurium(IV) Bromide |
10031-27-3 |
10g |
¥58900 |
2024-03-01 |
購入 |
富士フイルム和光純薬株式会社(wako)
|
W01SRM52-7000 |
臭化テルル(IV)
Tellurium(IV) Bromide |
10031-27-3 |
50g |
¥220600 |
2024-03-01 |
購入 |
テルル(IV)テトラブロミド 化学特性,用途語,生産方法
化学的特性
Yellow crystals. Soluble in a little water (decomposes in excess
water).
使用
Tellurium tetrabromide?it acts as a chemical and organic intermediate. It is also acts a conductor.
製造方法
Pure Te (5 g.) is introduced through adapter a into the elongated reaction flask A of the apparatus shown in Fig.1. Adapter a is connected to a N2 purification train which furnishes either pure dry N2 or N2 containing bromine vapor. For the latter, the gas stream may be passed through a wash bottle containing dry Br2 , followed by a U tube containing P2O5-glass wool. First, the apparatus in purged with pure N2. Then A is cooled with ice water and the N2 -Br2 mixture is introduced. A portion of the Br2 condenses on the Te and reacts quietly with it, while the remainder is retained in the empty U tube D, cooled with an ice-salt mixture. The difference between the weight loss of the Br2 wash bottle and the weight of the condensate in D indicates the amount of bromine remaining in A. When this becomes about twice the amount needed for quantitative conversion to TeBr4, the gas stream is interrupted, stopcock C is closed, and the product slurry is allowed to stand at room temperature for several hours (better overnight) in order to complete the reaction. Then C is reopened and the excess bromine is purged by a stream of N2 while A is simultaneously heated to 50℃. To purify the product, it is sublimed in vacuum. Gas inlet tube a is sealed off at d, the whole apparatus is tilted to a horizontal position, and ground glass joint E is connected to an aspirator through a P2O5 drying tube. During evacuation, A is heated to sublimation temperature (about 350℃) with an electric furnace. Any black condensate which may separate in B at 200℃ is vaporized by heating with a burner. The subsequently deposited yellow to orange-red powder is quite pure TeBr4; if necessary, this can be further purified by an analogous sublimation in high vacuum.
テルル(IV)テトラブロミド 上流と下流の製品情報
原材料
準備製品
テルル(IV)テトラブロミド 生産企業
Global( 65)Suppliers
10031-27-3(テルル(IV)テトラブロミド)キーワード:
- 10031-27-3
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- テルル(IV)テトラブロミド
- 臭化テルル(TeBr4)
- 臭化テルル(IV)
- 四臭化テルル
- 臭化テルル(Ⅳ)