1-(tert-ブトキシカルボニル)-3-ピペリドン
1-(tert-ブトキシカルボニル)-3-ピペリドン 物理性質
- 融点 :
- 35-40 °C (lit.)
- 沸点 :
- 289.8±33.0 °C(Predicted)
- 比重(密度) :
- 1.099±0.06 g/cm3(Predicted)
- 闪点 :
- >230 °F
- 貯蔵温度 :
- 2-8°C
- 酸解離定数(Pka):
- -1.71±0.20(Predicted)
- 外見 :
- 液体
- 色:
- 無色透明
- 水溶解度 :
- 水に不溶です。
- BRN :
- 5936353
- InChI:
- InChI=1S/C10H17NO3/c1-10(2,3)14-9(13)11-6-4-5-8(12)7-11/h4-7H2,1-3H3
- InChIKey:
- RIFXIGDBUBXKEI-UHFFFAOYSA-N
- SMILES:
- N1(C(OC(C)(C)C)=O)CCCC(=O)C1
- CAS データベース:
- 98977-36-7(CAS DataBase Reference)
1-(tert-ブトキシカルボニル)-3-ピペリドン 価格
もっと(20)
| メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01APOOR9057 |
Piperidin-3-one, N-BOC protected |
98977-36-7 |
5g |
￥5800 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01APOOR9057 |
Piperidin-3-one, N-BOC protected |
98977-36-7 |
25g |
￥6700 |
2024-03-01 |
購入 |
|
東京化成工業
|
B3309 |
1-(tert-ブトキシカルボニル)-3-ピペリドン >98.0%(GC)
1-(tert-Butoxycarbonyl)-3-piperidone
>98.0%(GC) |
98977-36-7 |
5g |
￥4100 |
2024-03-01 |
購入 |
|
東京化成工業
|
B3309 |
1-(tert-ブトキシカルボニル)-3-ピペリドン >98.0%(GC)
1-(tert-Butoxycarbonyl)-3-piperidone
>98.0%(GC) |
98977-36-7 |
25g |
￥13700 |
2024-03-01 |
購入 |
|
Sigma-Aldrich Japan
|
650811 |
1-Boc-3-ピペリドン 97%
1-Boc-3-piperidone 97% |
98977-36-7 |
25g |
￥19200 |
2024-03-01 |
購入 |
1-(tert-ブトキシカルボニル)-3-ピペリドン 化学特性,用途語,生産方法
外観
白色～橙黄色、固体または液体
化学的特性
White to yellow low melting solid
使用
1-Boc-3-piperidone, is used as an important raw material and intermediate used in organic Synthesis, pharmaceuticals, agrochemicals and dyestuff.
合成
With 179g compound 3(1-BOC-3-piperidines alcohol) drop in the 2L reaction flask, drop into pimelinketone 1300g, aluminum isopropylate 88g, methylene dichloride 400ml is warming up to 80 ℃, insulation reaction 8h, reaction finishes to be cooled to room temperature, adds 10% sodium hydroxide 200ml, stirring at normal temperature 30min, filter, the filtrate normal pressure reclaims methylene dichloride, reclaim under reduced pressure pimelinketone again, reclaim finish after, add the 300ml dichloromethane extraction three times, it is dry concentrated to merge oil reservoir, gets 1-BOC-3-piperidone crude product.
Refining: with 1-BOC-3-piperidone crude product is that 60pa, temperature are to distill under 104 ~ 105 ℃ the condition at pressure, gets 1-BOC-3-piperidone elaboration 163g, 92.9%.
1-(tert-ブトキシカルボニル)-3-ピペリドン 上流と下流の製品情報
原材料
準備製品
1-(tert-ブトキシカルボニル)-3-ピペリドン 生産企業
Global( 497)Suppliers
| 名前 |
電話番号 |
電子メール |
国籍 |
製品カタログ |
優位度 |
|
Chongqing Ensky Pharmaceutical Co.,Ltd.
|
+86-23-86815286 +86-13983794297
|
sales@ensky-chemical.com |
China |
87 |
58 |
|
Shanghai Quedan biology science and technology co., ltd
|
+86-13004146052
|
lnzc@quedan.com.cn |
China |
1060 |
58 |
|
Anhui Yisheng Technology Co., LTD
|
+86-19355901310 +86-19355901310
|
alice@ah-yisheng.com |
China |
333 |
58 |
|
Anhui Yiao New Material Technology Co., Ltd
|
+86-199-55145978 +8619955145978
|
sales8@anhuiyiao.com |
China |
253 |
58 |
|
Xiamen Wonderful Bio Technology Co., Ltd.
|
+8613043004613
|
Sara@xmwonderfulbio.com |
China |
305 |
58 |
|
Shandong Huisheng Import & Export Co., Ltd.
|
+86-13176845580 +86-13176845580
|
da@zhongda-biotech.com |
China |
248 |
58 |
|
Anhui Zhongda Biotechnology Co., Ltd
|
+8619956560829
|
justine@zhongda-biotech.com |
China |
300 |
58 |
|
Anhui Zhongda Biotechnology Co., Ltd
|
+8615689548120
|
linda@zhongda-biotech.com |
China |
204 |
58 |
|
Anhui Ruihan Technology Co., Ltd
|
+8617756083858
|
daisy@anhuiruihan.com |
China |
994 |
58 |
|
Capot Chemical Co.,Ltd.
|
571-85586718 +8613336195806
|
sales@capotchem.com |
China |
29797 |
60 |
1-(tert-ブトキシカルボニル)-3-ピペリドン スペクトルデータ(FT-IR)
98977-36-7(1-(tert-ブトキシカルボニル)-3-ピペリドン)キーワード:
- 98977-36-7
- T-BUTYL-3-PIPERIDONE-1-CARBOXYLATE
- 3-OXOPIPERIDINE, N-BOC PROTECTED
- 1-PIPERIDINECARBOXYLIC ACID, 3-OXO-, 1,1-DIMETHYLETHYL ESTER
- 1-N-BOC-3-PIPERIDONE
- 1-(TERT-BUTOXYCARBONYL)-3-PIPERIDINONE
- 1-BOC-3-PIPERIDONE
- 1-BOC-PIPERIDIN-3-ONE
- BOC-3-PIPERIDONE
- N-(TERT-BUTOXYCARBONYL)-3-PIPERIDINONE
- 3-ketopiperidine-1-carboxylic acid tert-butyl ester
- 3-oxo-1-piperidinecarboxylic acid tert-butyl ester
- 1-(tert-Butoxycarbonyl)-3-piperidone
- 1,1-Dimethylethyl 3-Oxo-1-Piperidine Carboxylate
- Tert-butyl-3-oxo-1-piperidinecarboxylate
- 1-Boc-3-piperidone,97%
- 1-N-TERT-BUTOXYCARBONYL-3-PIPERIDONE
- 3-Oxopiperidine, N-BOC protected 97%
- 1-N-Boc-piperdine-3-one
- N-BOC-3-piperidone,97%
- 1-N-Boc-3-Piperidine
- Piperidin-3-one, N-BOC protected 97%
- tert-Butyl 3-oxopiperidine-1-carboxylate, 3-Oxopiperidine, N-BOC protected
- N-(tert-Butoxycarbonyl)-3-piperidone
- 1-Boc-3-piperidone 97%
- N - bok - 3 - piperidine ketone
- 1-Boc-3-piperidone tert-Butyl 3-oxopiperidine-1-carboxylate
- 3-Oxopiperidine
- Piperidin-3-one, N-BOC protected
- 1-Boc-3-piperidone 98977-36-7
- 98977-36-7 tert-Butyl 3-oxopiperidine-1-carboxylate
- 1-(tert-ブトキシカルボニル)-3-ピペリドン
- 1-Boc-3-ピペリドン
- 3-オキソ-1-ピペリジンカルボン酸 tert-ブチル
- 1-BOC-3-ピペリジノン
- 1-N-BOC-3-ピペリドン