4-아이오도부틸아세테이트
|
|
4-아이오도부틸아세테이트 속성
- 끓는 점
- 94-95 °C5.5 mm Hg(lit.)
- 밀도
- 1.61 g/mL at 25 °C(lit.)
- 굴절률
- n
20/D 1.497(lit.)
- 인화점
- 195 °F
- 용해도
- 혼합하기가 어렵습니다.
- 물리적 상태
- 액체
- 색상
- Light green turbid
- 감도
- Light Sensitive
- CAS 데이터베이스
- 40596-44-9(CAS DataBase Reference)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
위험품 표기 | Xi | ||
---|---|---|---|
위험 카페고리 넘버 | 36/37/38 | ||
안전지침서 | 26-36/37/39 | ||
WGK 독일 | 3 | ||
HS 번호 | 29153900 |
4-아이오도부틸아세테이트 C화학적 특성, 용도, 생산
화학적 성질
CLEAR DARK BROWN LIQUID용도
4-Iodobutyl acetate is used in the preparation of tricyclohexyl(acetoxybutyl))phosphonium iodide, tri-n-hexyl(acetoxybutyl))phosphonium iodideSynthesis Reference(s)
Synthetic Communications, 24, p. 951, 1994 DOI: 10.1080/00397919408020770Synthesis
The synthesis of 4-IODOBUTYL ACETATE is as follows:Acetic acid (0.30mmol, 1.0 equivalent), CuI (0.03mmol, 10.0mol%, 5.7mg) and NaI (0.60mmol, 2.0 equivalent, 89.9mg) were added to a 10mL Schlenk tube equipped with a magnetic stirring device. Vacuum the flask with a pump and backfill it three times with nitrogen. Then, 1.0 mL tetrahydrofuran (12.30 mmol, 41.0 equivalence, 1 mL, c=0.30 M), deionized water (0.45 mmol, 1.5 equivalence) and TMSCF3 (0.36 mmol, 1.2 equivalence) were added under N2 atmosphere. The mixture is stirred at 150°C (thermostatic oil bath pot) for 12 hours. After cooling to room temperature, dilute the mixture with ethyl acetate (15 mL), wash with water and brine, and dry on anhydrousNa2SO4. After Extraction by EtOAc (5 mL x 3), the combined organic layer was dehydrated with anhydrousNa2SO4 and concentrated under reduced pressure. The crude product is purified by rapid chromatography on silica gel to obtain alkyl iodide.4-아이오도부틸아세테이트 준비 용품 및 원자재
원자재
준비 용품
4-아이오도부틸아세테이트 공급 업체
글로벌( 57)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
---|---|---|---|---|---|
Hebei Mojin Biotechnology Co., Ltd | +86 13288715578 +8613288715578 |
sales@hbmojin.com | China | 12465 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 |
sales@tnjchem.com | China | 34571 | 58 |
Nanjing Triumpharm Co.,Ltd | +86-02586182925 +86-15105172550 |
info@triumpharm.com | China | 129 | 58 |
SUZHOU SENFEIDA CHEMICAL CO.,LTD | +86-0512-83500002 +8615195660023 |
sales@senfeida.com | China | 23048 | 58 |
Aladdin Scientific | +1-+1(833)-552-7181 |
sales@aladdinsci.com | United States | 57511 | 58 |
Amadis Chemical Company Limited | 571-89925085 |
sales@amadischem.com | China | 131980 | 58 |
Mainchem Co., Ltd. | +86-0592-6210733 |
sale@mainchem.com | China | 32360 | 55 |
Wuhan Aikang Chemical Co., Ltd. | 13002132652 |
andriy@akkochemical.com | China | 279 | 58 |
Meryer (Shanghai) Chemical Technology Co., Ltd. | 021-61259108 18621169109 |
market03@meryer.com | China | 40240 | 62 |
Alfa Aesar | 400-6106006 |
saleschina@alfa-asia.com | China | 30132 | 84 |
4-아이오도부틸아세테이트 관련 검색:
2-iodo-1-ethanol acetate
3-iodo-1-propanol acetate
5-iodo-1-pentanol acetate
6-Iodo-1-Hexanol
5-Chloropentanol
6-Chlorohexanol
3-Bromo-1-propanol
6-iodo-1-hexanol acetate
8-iodo-1-octanol acetate
9-iodo-1-nonanol acetate
7-iodo-1-heptanol acetate
10-iodo-1-nonanol acetate
2-(acetoxymethyl)-4-iodobutyl acetate
4-IODOBUTYL ACETATE
1,2,3-TRI-O-BENZOYL-4-DEOXY-ALPHA-L-FUCOPYRANOSE
4-IODOBUTYL BENZOATE
8-(IODOMETHYL)-1,8-DIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE
2,3,5-TRI(ACETYLOXY)-6-(IODOMETHYL)TETRAHYDRO-2H-PYRAN-4-YL ACETATE