- [3-(1-Naphthyl)phenyl]boronic acid
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- $200.00 / 1KG
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2025-09-25
- CAS:881913-20-8
- Min. Order: 1KG
- Purity: 99%, 99.5% Sublimated
- Supply Ability: g-kg-tons, free sample is available
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| | BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]- Basic information |
| Product Name: | BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]- | | Synonyms: | BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]-;3-(Naphthalene-1-yl)-phenylboronic acid;(3-(Naphthalen-1-yl);3-(1-Naphthyl)benzeneboronic acid, 98%;3-(1-Naphthyl)phenylboronic Acid (contains varying amounts of Anhydride);3-(1-naphthalenyl)phenylboronic acid;3-(1-Naphthyl)benzeneboronic Acid (contains varying amounts of Anhydride);Boronic acid, B-[3-(1-naphthalenyl)phenyl]- | | CAS: | 881913-20-8 | | MF: | C16H13BO2 | | MW: | 248.08 | | EINECS: | | | Product Categories: | | | Mol File: | 881913-20-8.mol | ![BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]- Structure](CAS/GIF/881913-20-8.gif) |
| | BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]- Chemical Properties |
| Boiling point | 471.9±48.0 °C(Predicted) | | density | 1.23±0.1 g/cm3(Predicted) | | storage temp. | under inert gas (nitrogen or Argon) at 2-8°C | | pka | 8.27±0.19(Predicted) | | form | Powder | | color | Off-white | | CAS DataBase Reference | 881913-20-8 |
| | BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]- Usage And Synthesis |
| Uses | Boronic acid, [3-(1-naphthalenyl)phenyl]- | | Synthesis | General procedure for the synthesis of 3-(1-naphthyl)benzeneboronic acid from 1-bromonaphthalene and 1,3-phenylenediboronic acid: 1,3-phenylenediboronic acid (1.99 g, 12 mmol), 1-bromonaphthalene (2.07 g, 10 mmol), tetrakis(triphenylphosphine)palladium (0.58 g, 0.5 mmol) and potassium carbonate (4.15 g, 30 mmol) were dissolved in 100 mL of a THF:H2O (2:1) mixed solvent. The reaction was stirred at reflux for 2 h at 80 °C. After completion of the reaction, the organic layer was separated and extracted three times with ether (40 mL) and the organic phases were combined. The organic phase was dried with magnesium sulfate, filtered and the solvent was evaporated. The residue was purified by silica gel column chromatography to afford intermediate D-2 (1.74 g, 70% yield). | | References | [1] Patent: KR2016/30001, 2016, A. Location in patent: Paragraph 0368-0371 |
| | BORONIC ACID, [3-(1-NAPHTHALENYL)PHENYL]- Preparation Products And Raw materials |
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