Chlorendic anhydride(115-27-5) IR2
Product NameChlorendic anhydride
CAS115-27-5
Molecular FormulaC9H2Cl6O3
Molecular Weight370.83
InChIInChI=1S/C9H2Cl6O3/c10-3-4(11)8(13)2-1(5(16)18-6(2)17)7(3,12)9(8,14)15/h1-2H
InChIKey FLBJFXNAEMSXGL-UHFFFAOYSA-N
SmilesC1(=O)C2C(C3(Cl)C(Cl)(Cl)C2(Cl)C(Cl)=C3Cl)C(=O)O1
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MassMS2017-05387CM 1,4,5,6,7,7-hexachloro-5-norbornene-2,3-dicarboxylic anhydride C9H2Cl6O3 (Mass of molecular ion: 368)
Source Temperature: 245 °C Sample Temperature: 20 °C Direct, 70 eV
18.0 2.3 26.0 7.6 27.0 2.0 28.0 2.6 29.0 2.6 35.0 1.1 36.0 2.3 37.0 2.2 39.0 1.3 41.0 3.8 42.0 1.9 43.0 7.7 44.0 1.8 47.0 2.2 49.0 1.8 50.0 1.7 53.0 1.3 54.0 1.6 56.0 2.2 57.0 3.1 60.0 5.8 61.0 4.0 62.0 1.5 63.0 4.7 65.0 1.9 70.0 1.5 71.0 2.6 72.0 2.3 73.0 3.8 74.0 2.2 77.0 1.6 78.0 2.3 79.0 1.0 82.0 1.1 83.0 2.7 84.0 4.1 85.0 5.1 86.0 3.9 89.0 3.4 91.0 1.4 92.0 1.0 94.0 1.2 95.0 8.9 96.0 7.3 97.0 4.5 98.0 1.2 106.0 2.1 107.0 6.9 108.0 3.3 109.0 5.0 110.0 1.1 111.0 1.0 112.5 2.2 113.0 3.2 114.0 3.5 115.0 1.6 117.0 3.3 118.0 1.6 119.0 3.4 120.0 4.1 121.0 5.1 122.0 1.6 123.0 1.6 127.0 1.3 128.0 1.6 130.5 5.6 131.5 8.7 132.5 5.6 133.0 2.7 141.0 6.1 143.0 7.0 144.0 1.2 145.0 2.9 155.0 2.7 156.0 1.3 157.0 1.8 165.0 4.5 167.0 5.7 169.0 2.7 179.0 1.8 181.0 1.6 191.0 16.2 192.0 1.5 193.0 15.7 194.0 1.3 195.0 5.0 201.0 1.7 203.0 2.2 205.0 1.1 207.0 13.9 208.0 1.1 209.0 13.3 210.0 1.0 211.0 4.3 214.0 2.6 216.0 3.4 218.0 1.8 225.0 2.0 226.0 3.9 227.0 3.0 228.0 5.1 229.0 1.8 230.0 2.5 235.0 13.2 237.0 21.2 238.0 1.2 239.0 13.5 241.0 4.6 243.0 1.1 254.0 4.1 256.0 5.1 258.0 2.5 261.0 61.6 262.0 4.8 263.0 100.0 264.0 7.4 265.0 63.4 266.0 4.8 267.0 20.1 268.0 1.6 269.0 3.7 270.0 9.4 271.0 1.3 272.0 17.9 273.0 1.2 274.0 14.2 276.0 6.2 277.0 4.2 278.0 1.7 279.0 6.2 281.0 4.0 283.0 1.3 289.0 2.8 291.0 4.5 293.0 2.9 295.0 1.0 298.0 1.1 305.0 6.5 307.0 10.5 309.0 6.7 311.0 2.2 333.0 8.7 335.0 14.0 336.0 1.4 337.0 9.0 339.0 3.0 368.0 5.8 370.0 11.2 371.0 1.1 372.0 8.9 374.0 3.9
parameter in CDCl3
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1H NMR 300 MHz C9 H2 Cl6 O3 0.043 g : 0.5 ml CDCl3 1,4,5,6,7,7-hexachloro-5-norbornene-2,3-dicarboxylic anhydride 
Parameter ppm Hz
D(A) 4.154
Hz ppm Int.1246.20 4.154 1000
in DMSO-d6
CCl4 solution
KBr disk
Nujol
