1,4-ANHYDRO-D-GLUCITOL(27299-12-3) IR1

Product Name1,4-ANHYDRO-D-GLUCITOL

CAS 27299-12-3

Molecular FormulaC6H12O5

Molecular Weight164.16

Request For Quotation

Mass

MS-NW-6968          
1,4-anhydro-D-glucitol
C6H12O5             (Mass of molecular ion:    164)

   Source Temperature: 200 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      14.0       1.3
      15.0      14.7
      17.0       1.3
      18.0       5.7
      19.0      20.6
      26.0       2.4
      27.0      19.3
      28.0      17.5
      29.0      31.6
      30.0       3.8
      31.0      49.7
      32.0       1.3
      39.0       7.1
      40.0       3.8
      41.0      13.8
      42.0      10.9
      43.0      71.7
      44.0      38.9
      45.0      71.8
      46.0       2.4
      47.0       3.9
      53.0       1.2
      54.0       1.4
      55.0      22.4
      56.0      26.0
      57.0      64.6
      58.0      26.4
      59.0       8.6
      60.0      26.5
      61.0      55.3
      62.0       1.9
      68.0       1.4
      69.0      25.5
      70.0       1.8
      71.0      10.3
      72.0       1.9
      73.0      83.8
      74.0      17.1
      75.0       5.0
      82.0       1.0
      84.0       2.1
      85.0      20.3
      86.0     100.0
      87.0       8.6
      88.0       1.0
      89.0       1.0
      91.0       1.9
      97.0       2.0
      98.0       1.8
      99.0       2.4
     102.0       1.7
     103.0      93.1
     104.0       5.8
     105.0       1.4
     111.0       2.4
     115.0       3.2
     116.0       1.1
     128.0       3.2
     133.0       7.2
     146.0       4.7

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₁₂ O₅	0.039 g : 0.5 ml DMSO-d₆
1,4-anhydro-D-glucitol

    Assign.     Shift(ppm)

      A     *1      5.00
      B     *1      4.82
      C             4.50
      D             4.37
      E             3.95
      F             3.91
      G     *2      3.90
      J             3.64
      L     *3      3.567
      M     *2      3.440
      N     *3      3.36

     Hz     ppm     Int.

   2001.71   5.009    830
   1998.54   5.001    831
   1929.44   4.828    977
   1925.17   4.818    979
   1800.66   4.506    603
   1798.34   4.500    372
   1795.29   4.493    570
   1788.82   4.476     30
   1750.85   4.381    431
   1745.00   4.367    971
   1739.26   4.352    451
   1582.89   3.961    260
   1579.10   3.952    500
   1575.56   3.943    353
   1566.89   3.921    742
   1563.11   3.912    611
   1558.11   3.899    480
   1554.08   3.889    319
   1470.70   3.680     39
   1468.14   3.674     35
   1465.21   3.667     38
   1462.16   3.659    197
   1459.47   3.652    314
   1454.96   3.641   1000
   1446.78   3.621     80
   1443.24   3.612     44
   1435.55   3.593    174
   1434.94   3.591    172
   1429.69   3.578    177
   1428.83   3.576    172
   1424.56   3.565    257
   1422.12   3.559    227
   1418.82   3.551    241
   1416.38   3.545    212
   1379.39   3.452    665
   1370.36   3.429    622
   1363.89   3.413     38
   1362.67   3.410     35
   1362.06   3.409     37
   1353.03   3.386    150
   1346.92   3.371    261
   1341.55   3.357    229
   1335.82   3.343    235
   1329.96   3.328    114

D2O

in DMSO-d6