5-Decanone, 6-hydroxy-(27620-76-4) MS
Product Name5-Decanone, 6-hydroxy-
CAS27620-76-4
Molecular FormulaC10H20O2
Molecular Weight172.26
-
MassMS-NW-6640 valeroin C10H20O2 (Mass of molecular ion: 172)
Source Temperature: 210 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 2.3 27.0 11.2 28.0 1.6 29.0 19.2 31.0 4.3 39.0 5.3 41.0 37.4 42.0 2.7 43.0 11.6 44.0 3.6 45.0 7.7 53.0 1.2 55.0 6.5 56.0 1.6 57.0 45.0 58.0 2.9 60.0 4.1 67.0 1.3 69.0 100.0 70.0 6.3 71.0 1.4 73.0 2.7 74.0 2.0 83.0 2.5 84.0 1.4 85.0 48.9 86.0 15.7 87.0 41.3 88.0 2.5 97.0 2.3 99.0 1.9 100.0 1.2 113.0 1.5 114.0 1.7 116.0 4.2 155.0 1.8 156.0 5.1 241.0 1.0
400 MHz in CDCl3
-
1H NMR 399.65 MHz C10 H20 O2 0.05 ml : 0.5 ml CDCl3 valeroin 
Assign. Shift(ppm)
A 4.175 B 3.60 C *1 2.496 D *1 2.454 E 1.825 F 1.61 G 1.49 J 1.33 K *2 0.920 L *2 0.914
Hz ppm Int.1673.83 4.189 84 1670.41 4.180 96 1666.63 4.171 87 1662.84 4.161 79 1437.26 3.597 50 999.88 2.502 115 992.07 2.483 265 984.50 2.464 289 976.93 2.445 118 732.91 1.834 63 732.42 1.833 61 729.13 1.825 61 722.66 1.809 64 718.87 1.799 65 658.94 1.649 68 651.61 1.631 174 649.41 1.625 82 649.17 1.625 82 643.80 1.611 231 641.72 1.606 121 636.23 1.592 207 628.66 1.574 107 618.65 1.548 70 616.21 1.542 68 612.92 1.534 61 608.28 1.523 70 587.04 1.469 62 585.08 1.464 72 579.71 1.451 63 578.13 1.447 60 569.34 1.425 74 560.91 1.404 66 559.08 1.399 60 556.03 1.392 95 553.22 1.385 102 549.19 1.375 135 547.36 1.370 157 545.78 1.366 218 540.04 1.352 261 538.45 1.348 333 532.84 1.334 291 530.76 1.329 292 526.12 1.317 145 523.19 1.310 204 517.82 1.296 74 517.46 1.295 74 515.99 1.292 86 375.37 0.940 561 372.56 0.933 422 367.92 0.921 1000 365.48 0.915 669 360.60 0.903 518 358.40 0.897 314
in CDCl3
liquid film
