endo-2-Norbornanamine(31002-73-0) IR1

Product Nameendo-2-Norbornanamine

CAS 31002-73-0

Molecular FormulaC7H13N

Molecular Weight111.18

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Mass

MS-NW-9711          
endo-2-norbornanamine hydrochloride
C7H13N HCl          (Mass of molecular ion:    111)

   Source Temperature: 160 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       2.3
      27.0       2.9
      28.0       7.9
      29.0       1.7
      30.0      16.2
      35.0       3.0
      36.0      29.8
      37.0       1.1
      38.0      10.5
      39.0       6.9
      40.0       1.4
      41.0       8.8
      42.0       7.4
      43.0      33.6
      44.0       7.8
      45.0      15.6
      51.0       1.5
      52.0       1.0
      53.0       3.6
      54.0       3.7
      55.0       3.1
      56.0      50.3
      57.0      14.3
      65.0       5.1
      66.0      17.3
      67.0      17.5
      68.0       5.0
      69.0      12.9
      70.0      27.7
      71.0       1.4
      77.0       5.3
      78.0       2.5
      79.0      56.9
      80.0       7.0
      81.0       3.1
      82.0     100.0
      83.0      18.6
      84.0       1.0
      91.0       3.1
      93.0       4.7
      94.0      47.6
      95.0       4.4
      96.0      10.7
     110.0       8.7
     111.0      45.9
     112.0       4.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₃ N	0.039 g : 0.5 ml CDCl₃
endo-2-norbornanamine hydrochloride

    Assign.     Shift(ppm)

      A             8.43
      B             3.561
      C             2.61
      D             2.297
      E     *1      2.052
      F     *2      1.86
      G             1.60
      J     *2      1.55
      K             1.42
      L     *1      1.260
     
     ASSIGNED BY C-H COSY

     Hz     ppm     Int.

   3368.41   8.429    403
   1432.98   3.586    116
   1428.96   3.576    229
   1424.56   3.565    151
   1422.49   3.560    158
   1417.85   3.548    244
   1413.94   3.538    138
   1042.36   2.609    396
    918.21   2.298    374
    836.06   2.092     93
    833.62   2.086    100
    831.42   2.081    102
    828.98   2.075     91
    825.07   2.065    108
    822.63   2.059    201
    820.31   2.053    210
    817.99   2.047    195
    815.80   2.042    113
    811.77   2.032    111
    809.20   2.025    112
    807.01   2.020    111
    804.57   2.014     92
    755.37   1.891     76
    753.42   1.886     66
    753.05   1.885     66
    752.81   1.884     66
    752.56   1.884     66
    745.61   1.866    268
    735.84   1.842    123
    735.35   1.840    124
    730.22   1.828    101
    662.23   1.658     31
    655.76   1.641     90
    652.10   1.632    144
    648.56   1.623    150
    643.31   1.610    386
    640.50   1.603    418
    631.59   1.581    404
    629.52   1.576    481
    617.07   1.545    235
    611.57   1.531    134
    580.08   1.452     52
    579.22   1.450     54
    568.36   1.423   1000
    557.86   1.396     72
    556.27   1.392     78
    513.06   1.284    183
    510.99   1.279    200
    509.03   1.274    206
    506.96   1.269    180
    503.17   1.260     36
    499.63   1.251    173
    497.56   1.245    188
    495.61   1.241    195
    493.65   1.236    169

in CDCl3

KBr disc

nujol mull

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