(4S,5S)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine(35019-66-0) MS
Product Name(4S,5S)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine
CAS35019-66-0
Molecular FormulaC12H17NO2
Molecular Weight207.27
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MassMS-NW-7612 (4S,5S)-(+)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine C12H17NO2 (Mass of molecular ion: 207)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.7 18.0 1.7 27.0 1.1 28.0 2.0 29.0 1.2 30.0 1.8 39.0 2.1 41.0 2.2 42.0 6.9 43.0 100.0 44.0 4.4 50.0 1.0 51.0 2.6 58.0 2.2 59.0 1.5 63.0 1.0 65.0 1.5 77.0 4.9 78.0 1.1 79.0 1.0 83.0 1.4 89.0 1.4 90.0 1.9 91.0 6.8 92.0 1.5 100.0 1.2 101.0 3.9 103.0 2.6 104.0 1.4 105.0 2.8 106.0 1.4 117.0 2.5 118.0 3.9 119.0 5.3 120.0 1.9 130.0 1.3 131.0 1.0 132.0 5.2 133.0 1.2 144.0 1.7 149.0 1.1 159.0 1.3 192.0 1.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C12 H17 N O2 0.05 ml : 0.5 ml CDCl3 (4S,5S)-(+)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine 
Assign. Shift(ppm)
A 7.39 to 7.18 B 5.061 C *1 4.238 D *1 3.871 E 2.704 F 1.520 G 1.44 J(B,E)=1.8HZ J(C,D)=-11.7HZ J(C,E)=1.8HZ J(D,E)=2.3HZ
Hz ppm Int.662.00 7.392 31 659.38 7.363 71 657.56 7.343 116 654.94 7.313 591 648.13 7.237 35 646.13 7.215 30 646.00 7.214 30 454.25 5.073 94 452.44 5.052 92 388.31 4.336 42 386.00 4.310 44 376.63 4.206 80 374.31 4.180 78 351.81 3.929 87 350.00 3.908 88 340.13 3.798 49 338.31 3.778 49 245.19 2.738 39 243.31 2.717 86 241.13 2.693 82 239.19 2.671 37 136.19 1.521 1000 128.75 1.438 294
in CDCl3
liquid film
