D-(+)-Norephedrine(37577-28-9) MS
Product NameD-(+)-Norephedrine
CAS37577-28-9
Molecular FormulaC9H13NO
Molecular Weight151.21
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MassMS-IW-9093 (1S,2R)-(+)-2-amino-1-phenyl-1-propanol C9H13NO (Mass of molecular ion: 151)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 5.9 27.0 1.5 28.0 2.5 39.0 2.5 41.0 1.1 42.0 12.7 43.0 1.8 44.0 100.0 45.0 3.0 50.0 1.7 51.0 4.4 52.0 1.3 56.0 1.1 63.0 1.5 65.0 2.6 70.0 1.6 71.0 2.1 77.0 8.7 78.0 2.0 79.0 4.4 89.0 1.6 90.0 1.2 91.0 12.6 92.0 13.6 93.0 1.1 104.0 1.2 105.0 5.5 106.0 3.5 107.0 2.1 115.0 2.2 116.0 1.6 117.0 4.0 118.0 2.6 132.0 8.0 133.0 8.2 134.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H13 N O 0.041 g : 0.5 ml CDCl3 (1S,2R)-(+)-2-amino-1-phenyl-1-propanol 
Assign. Shift(ppm)
A 7.31 B 7.26 C 4.429 D 3.057 E 2.3 F 0.925
Hz ppm Int.2930.54 7.333 70 2929.32 7.330 105 2927.73 7.326 45 2923.34 7.315 191 2922.12 7.312 282 2920.90 7.309 224 2917.48 7.301 115 2915.16 7.295 416 2909.67 7.281 293 2907.96 7.277 547 2905.40 7.270 153 2903.93 7.267 197 2902.95 7.264 225 2901.37 7.260 267 2898.44 7.253 104 2895.75 7.246 200 2892.70 7.239 45 2890.87 7.234 42 2888.92 7.229 64 2887.21 7.225 33 1772.46 4.436 246 1767.58 4.423 255 1234.01 3.088 37 1229.00 3.076 50 1227.42 3.072 127 1222.53 3.060 133 1220.95 3.056 137 1216.06 3.043 129 1214.60 3.040 53 1209.59 3.027 39 930.05 2.328 34 372.92 0.934 982 366.33 0.917 1000
in CDCl3
KBr disc
nujol mull
