6-(beta-Hydroxyethylamino)-purine(4551-95-5) MS
Product Name6-(beta-Hydroxyethylamino)-purine
CAS4551-95-5
Molecular FormulaC7H9N5O
Molecular Weight179.18
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MassMS-NW-7974 6-(2-hydroxyethylamino)purine C7H9N5O (Mass of molecular ion: 179)
Source Temperature: 210 °C Sample Temperature: 170 °C Direct, 75 eV
15.0 2.0 18.0 4.5 19.0 1.0 27.0 4.0 28.0 28.7 29.0 2.6 30.0 44.6 31.0 3.2 38.0 3.2 39.0 4.1 40.0 5.8 41.0 3.3 42.0 2.7 43.0 3.6 44.0 1.5 45.0 2.0 52.0 2.3 53.0 6.7 54.0 3.5 55.0 1.6 64.0 1.6 65.0 9.3 66.0 10.1 67.0 7.3 68.0 1.1 77.0 1.3 79.0 1.6 80.0 1.9 81.0 1.7 91.0 1.0 92.0 11.8 93.0 12.7 94.0 7.8 106.0 1.1 107.0 1.1 108.0 7.3 119.0 36.3 120.0 13.8 121.0 15.8 122.0 1.3 134.0 1.2 135.0 22.8 136.0 16.1 137.0 1.2 148.0 100.0 149.0 59.4 150.0 4.9 160.0 8.9 161.0 2.4 162.0 1.5 179.0 14.6 180.0 2.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H9 N5 O 0.031 g : 0.5 ml DMSO-d6 6-(2-hydroxyethylamino)purine 
Assign. Shift(ppm)
A 12.9 B 8.229 C 8.145 D 7.51 E 4.88 F 3.62 ASSIGNED BY C-H COSY
Hz ppm Int.3288.81 8.230 369 3255.69 8.147 895 3001.19 7.510 164 1948.58 4.876 55 1469.29 3.677 31 1468.44 3.675 32 1449.21 3.627 1000 1420.14 3.554 87
in DMSO-d6
KBr disc
nujol mull
