3-Heptafluorobutyryl-(+)-camphor(51800-99-8) MS
Product Name3-Heptafluorobutyryl-(+)-camphor
CAS51800-99-8
Molecular FormulaC14H15F7O2
Molecular Weight348.26
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MassMS-NW-7728 3-heptafluorobutyryl-(+)-camphor C14H15F7O2 (Mass of molecular ion: 348)
Source Temperature: 130 °C Sample Temperature: 100 °C Direct, 75 eV
18.0 3.2 27.0 10.2 28.0 1.9 29.0 8.8 31.0 1.0 39.0 16.0 40.0 3.3 41.0 42.1 42.0 2.6 43.0 23.4 45.0 3.3 50.0 1.3 51.0 4.5 52.0 2.3 53.0 10.3 54.0 2.7 55.0 28.8 56.0 2.4 57.0 5.3 59.0 2.5 63.0 1.6 65.0 5.4 66.0 2.4 67.0 13.3 68.0 3.9 69.0 14.8 70.0 3.1 71.0 1.3 75.0 1.4 77.0 9.3 78.0 3.0 79.0 9.4 80.0 4.3 81.0 10.0 82.0 4.1 83.0 20.2 84.0 5.4 90.0 1.1 91.0 12.6 92.0 2.0 93.0 7.3 94.0 2.7 95.0 31.2 96.0 3.7 97.0 2.3 100.0 2.2 103.0 1.1 105.0 4.1 106.0 1.2 107.0 8.0 108.0 20.2 109.0 11.8 110.0 2.8 115.0 1.0 117.0 1.6 118.0 1.0 119.0 22.2 120.0 2.3 121.0 4.7 122.0 4.7 123.0 26.3 124.0 3.1 131.0 1.2 133.0 10.4 134.0 1.4 135.0 9.4 136.0 7.8 137.0 5.1 139.0 1.1 145.0 1.0 146.0 1.0 149.0 1.8 150.0 1.7 151.0 50.7 152.0 6.4 153.0 1.0 159.0 1.0 161.0 3.0 164.0 1.3 169.0 5.0 179.0 12.9 180.0 1.5 181.0 1.8 201.0 1.3 209.0 1.0 249.0 1.0 251.0 1.1 259.0 1.1 263.0 1.5 264.0 1.2 265.0 5.1 273.0 1.2 277.0 4.0 278.0 1.3 279.0 1.2 285.0 2.1 287.0 2.4 291.0 4.1 292.0 1.2 293.0 1.1 300.0 4.7 301.0 5.2 302.0 2.4 304.0 1.8 305.0 27.1 306.0 9.1 307.0 1.4 315.0 2.6 319.0 1.7 320.0 43.1 321.0 6.3 329.0 1.0 333.0 26.6 334.0 3.9 348.0 100.0 349.0 16.3 350.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H15 F7 O2 0.05 ml : 0.5 ml CDCl3 3-heptafluorobutyryl-(+)-camphor 
Assign. Shift(ppm)
A 12. B 2.870 C 2.09 D 1.78 E 1.48 F 1.45 G 1.020 J 0.976 K 0.832 ASSIGNED BY C-H COSY.
Hz ppm Int.1147.27 2.871 70 1146.84 2.870 70 1141.50 2.857 39 840.85 2.104 49 837.00 2.095 65 832.94 2.085 30 829.52 2.076 30 825.46 2.066 50 730.37 1.828 42 727.17 1.820 45 717.55 1.796 55 715.84 1.792 49 714.35 1.788 61 706.23 1.768 44 607.72 1.521 32 598.53 1.498 62 594.68 1.489 86 588.06 1.472 115 585.92 1.467 141 580.37 1.453 73 577.16 1.445 59 408.14 1.022 1000 390.40 0.977 827 385.49 0.965 41 332.92 0.834 744
in CDCl3
liquid film
4880 A,200 M,liquid
