ethyl N-(4-chlorophenyl)-2-oxoglycinate (5397-14-8) IR1
Product Nameethyl N-(4-chlorophenyl)-2-oxoglycinate
CAS5397-14-8
Molecular FormulaC10H10ClNO3
Molecular Weight227.64
-
MassMS-NW-8061 ethyl 4'-chlorooxanilate C10H10ClNO3 (Mass of molecular ion: 227)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 2.4 26.0 1.0 27.0 9.2 28.0 4.4 29.0 72.7 30.0 2.1 37.0 1.1 38.0 2.7 39.0 3.9 45.0 6.1 45.5 2.3 50.0 4.9 51.0 2.7 52.0 1.6 61.0 1.4 62.0 3.4 63.0 10.9 64.0 5.6 65.0 3.7 73.0 7.3 74.0 3.6 75.0 16.6 76.0 4.1 77.0 1.8 85.0 1.4 89.0 1.4 90.0 9.0 91.0 6.4 92.0 3.3 93.0 1.0 99.0 20.6 100.0 4.6 101.0 6.9 102.0 1.6 105.0 1.0 111.0 18.2 112.0 2.0 113.0 6.4 119.0 1.5 120.0 1.9 125.0 6.2 126.0 70.8 127.0 36.8 128.0 25.6 129.0 11.3 130.0 1.0 139.0 1.8 140.0 14.2 141.0 1.7 142.0 4.6 153.0 70.9 154.0 88.5 155.0 37.9 156.0 29.5 157.0 5.1 227.0 100.0 228.0 12.3 229.0 33.1 230.0 4.0
400 MHz in CDCl3
-
1H NMR 399.65 MHz C10 H10 Cl N O3 0.030 g : 0.5 ml CDCl3 ethyl 4'-chlorooxanilate 
Assign. Shift(ppm)
A 8.96 B 7.615 C 7.339 D 4.410 E 1.417
Hz ppm Int.3579.47 8.957 73 3051.27 7.635 54 3048.34 7.628 436 3046.26 7.623 161 3041.50 7.611 170 3039.43 7.606 521 3036.38 7.598 77 2940.19 7.357 68 2937.26 7.350 505 2935.18 7.345 172 2930.42 7.333 157 2928.34 7.328 432 2925.42 7.320 61 1773.68 4.439 156 1766.48 4.421 480 1759.28 4.403 488 1752.20 4.385 168 573.73 1.436 491 566.53 1.418 1000 559.33 1.400 496
in CDCl3
KBr disc
nujol mull
