N,N'-bis(2-hydroxy-alpha-methylbenzylidene)ethylenediamine(5464-60-8) IR2

Mass

MS-IW-0001          
N,N'-bis(2-hydroxy-alpha-methylbenzylidene)ethylenediamine
C18H20N2O2          (Mass of molecular ion:    296)

   Source Temperature: 230 °C
   Sample Temperature: 180 °C
   Direct, 75 eV

      30.0       2.9
      39.0       2.8
      42.0       4.2
      44.0       1.2
      51.0       1.4
      63.0       1.4
      64.0       1.0
      65.0       5.0
      77.0       4.8
      78.0       1.4
      79.0       1.8
      89.0       1.2
      90.0       1.3
      91.0      12.7
      92.0       1.8
     102.0       1.0
     105.0       1.0
     107.0      18.3
     108.0       1.6
     118.0       1.1
     119.0       7.1
     120.0       5.7
     121.0       1.6
     132.0       5.3
     133.0       3.1
     134.0       2.1
     135.0       8.7
     136.0      18.2
     137.0       1.7
     144.0       2.7
     146.0      14.2
     147.0       2.3
     148.0      27.8
     149.0       6.5
     150.0       4.9
     160.0      24.0
     161.0      70.1
     162.0      17.1
     163.0       2.3
     221.0       1.6
     236.0       8.2
     237.0       1.9
     279.0       1.2
     281.0       3.0
     295.0       1.0
     296.0     100.0
     297.0      25.1
     298.0       3.4

Assign. Shift(ppm) A 15.6 B 7.490 C 7.243 D 6.894 E 6.739 F 3.948 G 2.346

     Hz     ppm     Int.

   6232.18  15.595     40
   2998.78   7.504    100
   2997.07   7.500    105
   2990.72   7.484    108
   2989.01   7.480    111
   2904.05   7.267     59
   2902.59   7.263     62
   2896.97   7.249     75
   2895.51   7.246    104
   2894.29   7.243     84
   2888.67   7.229     78
   2886.96   7.224     75
   2760.01   6.907    132
   2758.79   6.904    139
   2751.71   6.886    121
   2750.49   6.883    124
   2709.72   6.781     78
   2708.50   6.778     83
   2702.64   6.763     88
   2701.42   6.760    125
   2700.44   6.758     91
   2694.58   6.743     75
   2693.36   6.740     75
   1577.88   3.949    542
    937.99   2.348   1000