2,2,6,6-TETRACHLOROCYCLOHEXANOL(56207-45-5) IR1

Mass

MS-NW-7505          
2,2,6,6-tetrachlorocyclohexanol
C6H8Cl4O            (Mass of molecular ion:    236)

   Source Temperature: 260 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      18.0       1.3
      26.0       2.5
      27.0      14.2
      28.0       3.6
      29.0       8.3
      31.0       2.5
      35.0       1.2
      36.0       7.4
      37.0       1.3
      38.0       3.3
      39.0      22.2
      40.0       3.9
      41.0      19.9
      42.0       1.3
      43.0       1.5
      44.0       1.7
      47.0       1.7
      48.0       1.1
      49.0       4.5
      50.0       3.1
      51.0       5.5
      52.0       1.0
      53.0       2.6
      55.0       3.8
      57.0       3.7
      61.0       5.5
      62.0       1.6
      63.0       7.4
      64.0       1.0
      65.0      17.1
      66.0       2.1
      67.0       3.9
      69.0       2.7
      73.0       3.4
      74.0       1.1
      75.0      19.6
      76.0       4.9
      77.0       7.6
      78.0       3.5
      83.0       1.9
      85.0       1.7
      87.0       2.5
      89.0       2.4
      91.0     100.0
      92.0       3.8
      93.0      31.8
      94.0       1.5
      95.0       1.2
      96.0       3.4
      97.0       1.1
      98.0       2.2
      99.0       2.2
     101.0      24.8
     102.0       2.2
     103.0       9.5
     104.0       9.1
     105.0       2.6
     106.0       3.0
     109.0      11.8
     110.0      20.3
     111.0       9.1
     112.0      15.7
     113.0       2.2
     114.0       4.2
     117.0       1.2
     122.0      24.0
     123.0       2.2
     124.0      14.6
     125.0       4.7
     126.0       2.7
     127.0       2.6
     129.0       5.1
     130.0       1.1
     131.0       2.0
     135.0       3.4
     136.0      15.6
     137.0       6.9
     138.0      10.5
     139.0       3.9
     140.0       2.1
     143.0       1.6
     145.0       1.4
     147.0       2.3
     149.0       1.5
     165.0       4.9
     167.0       3.0
     169.0       4.0
     170.0       6.1
     171.0       3.7
     172.0       6.1
     173.0       1.6
     174.0       2.1
     183.0       8.2
     185.0       7.6
     187.0       2.8
     200.0       3.7
     201.0       6.3
     202.0       3.8
     203.0       5.8
     204.0       1.5
     205.0       2.0
     220.0       1.0

Assign. Shift(ppm) A 4.186 B 3.18 C 2.797 D 2.361 E 2.009 F 1.756 J(A,B)=10.5HZ 90MHZ : HSP-06-093

     Hz     ppm     Int.

   1678.59   4.201    937
   1673.71   4.188     36
   1668.09   4.174    992
   1274.05   3.188   1000
   1269.53   3.177     35
   1269.17   3.176     35
   1268.55   3.175     34
   1263.55   3.162    950
   1129.64   2.827    325
   1128.05   2.823    318
   1126.34   2.819    547
   1123.17   2.811    354
   1122.19   2.808    243
   1114.87   2.790    407
   1113.04   2.786    440
   1111.69   2.782    647
   1109.62   2.777    357
   1108.40   2.774    395
   1102.66   2.760     44
   1101.44   2.757     40
   1100.83   2.755     40
    959.96   2.403    266
    958.98   2.400    260
    956.30   2.393    285
    955.32   2.391    266
    948.00   2.373    220
    946.66   2.369    488
    945.80   2.367    479
    944.58   2.364    406
    942.87   2.360    526
    942.14   2.358    492
    937.13   2.345     51
    936.89   2.345     51
    933.23   2.336    232
    932.13   2.333    329
    930.91   2.330    220
    929.44   2.326    252
    928.47   2.324    304
    927.25   2.321    200
    826.42   2.068     83
    823.49   2.061    158
    820.43   2.053     89
    813.96   2.037     85
    811.65   2.031    147
    810.30   2.028    275
    808.72   2.024    241
    806.76   2.019    113
    805.79   2.017    130
    799.19   2.000    127
    797.24   1.995    166
    795.53   1.991    343
    794.31   1.988    123
    793.21   1.985    127
    792.11   1.983    110
    785.40   1.966     89
    782.47   1.958    150
    779.42   1.951     78
    715.58   1.791    100
    711.91   1.782    318
    708.37   1.773    468
    704.71   1.764    329
    700.93   1.754    170
    697.27   1.745    267
    693.60   1.736    362
    689.94   1.727    243
    686.40   1.718     83