3-(dipropylamino)propane-1,2-diol(60302-96-7) 1H NMR
Product Name3-(dipropylamino)propane-1,2-diol
CAS60302-96-7
Molecular FormulaC9H21NO2
Molecular Weight175.27
-
MassMS-NW-8525 3-dipropylamino-1,2-propanediol C9H21NO2 (Mass of molecular ion: 175)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
15.0 2.6 18.0 1.1 19.0 1.1 27.0 9.8 28.0 4.8 29.0 3.8 30.0 31.9 31.0 3.9 39.0 2.7 41.0 15.5 42.0 19.2 43.0 28.9 44.0 12.2 45.0 1.5 56.0 3.6 57.0 3.2 58.0 2.9 60.0 7.9 70.0 4.9 72.0 26.7 73.0 1.4 84.0 2.6 86.0 22.1 87.0 1.4 102.0 3.8 114.0 100.0 115.0 8.3 128.0 1.4 144.0 13.0 145.0 1.2 146.0 7.4
400 MHz in CDCl3
-
1H NMR 399.65 MHz C9 H21 N O2 0.05 ml : 0.5 ml CDCl3 3-dipropylamino-1,2-propanediol 
Assign. Shift(ppm)
A 3.90 B 3.735 C *1 3.691 D *1 3.506 E *2 2.552 F *3 2.46 G *2 2.43 J *3 2.42 K *4 1.49 L *4 1.45 M 0.881 J(C,D) = -11.1 HZ J(B,D) = 4.5 HZ J(B,C) = 4.0 HZ J(E,G) = -12.7 HZ J(E,B) = 8.9 HZ J(B,G) = 4.5 HZ J(F,J) = -12.8 HZ J(F,L) = 8.7 HZ J(F,K) = 7.1 HZ J(J,K) = 8.5 HZ J(J,L) = 5.7 HZ
Hz ppm Int.1559.45 3.903 38 1498.54 3.750 63 1494.14 3.739 90 1489.75 3.728 90 1485.47 3.717 80 1482.91 3.711 128 1482.06 3.709 132 1479.00 3.701 55 1471.92 3.684 142 1467.90 3.673 104 1408.69 3.525 90 1404.17 3.514 113 1397.58 3.498 97 1393.07 3.486 70 1032.96 2.585 67 1024.05 2.563 72 1020.26 2.553 127 1011.35 2.531 128 1000.61 2.504 55 993.77 2.487 73 991.94 2.483 65 987.79 2.472 154 984.86 2.465 82 981.08 2.455 186 979.13 2.450 270 976.56 2.444 193 974.73 2.439 163 972.05 2.433 193 970.70 2.429 205 967.65 2.422 182 966.67 2.419 155 963.62 2.412 94 962.04 2.408 240 957.76 2.397 55 954.96 2.390 74 949.22 2.376 55 610.35 1.528 49 608.64 1.523 38 607.18 1.520 33 602.91 1.509 111 601.68 1.506 77 599.85 1.501 50 595.46 1.490 159 594.12 1.487 133 588.99 1.474 197 588.13 1.472 191 581.67 1.456 147 580.44 1.453 190 573.24 1.435 119 566.77 1.419 43 566.16 1.417 43 359.38 0.900 594 352.05 0.881 1000 344.48 0.862 528
in CDCl3
liquid film
4880 A,200 M,liquid
