Dichlorodiphenylsilane(80-10-4) Raman

Product NameDichlorodiphenylsilane

CAS 80-10-4

Molecular FormulaC12H10Cl2Si

Molecular Weight253.2

InChIInChI=1S/C12H10Cl2Si/c13-15(14,11-7-3-1-4-8-11)12-9-5-2-6-10-12/h1-10H

InChIKey OSXYHAQZDCICNX-UHFFFAOYSA-N

Smiles[Si](C1=CC=CC=C1)(C1=CC=CC=C1)(Cl)Cl

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Mass

MS-NW-5281          
dichlorodiphenylsilane
C12H10Cl2Si         (Mass of molecular ion:    252)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       1.2
      39.0       1.6
      50.0       5.1
      51.0      15.4
      52.0       1.4
      53.0       1.7
      63.0      15.9
      65.0       5.7
      74.0       1.8
      75.0       1.8
      76.0       4.6
      77.0      28.0
      78.0       3.0
     108.0       6.6
     108.5       1.5
     109.0       2.5
     123.0       1.7
     125.0       1.1
     139.0       3.0
     140.0       1.0
     141.0       1.4
     151.0       1.6
     152.0       5.6
     153.0       5.4
     154.0     100.0
     155.0      13.3
     174.0       1.6
     175.0      35.2
     176.0       5.3
     177.0      23.5
     178.0       3.0
     179.0       4.6
     180.0       1.0
     181.0       2.3
     215.0       9.8
     216.0       7.6
     217.0      10.2
     218.0       3.7
     219.0       2.7
     251.0       2.6
     252.0      34.4
     253.0       7.9
     254.0      23.4
     255.0       4.7
     256.0       4.7

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₂ H₁₀ Cl₂ Si	0.04 ml : 0.5 ml CDCl₃
dichlorodiphenylsilane

    Assign.     Shift(ppm)

      A             7.74
      B             7.51
      C             7.47

     Hz     ppm     Int.

    701.31   7.831     52
    700.19   7.819     44
    698.63   7.801    452
    696.44   7.777    597
    695.19   7.763    154
    693.75   7.747    410
    692.31   7.731    508
    691.88   7.726    373
    691.31   7.719    314
    690.00   7.705    415
    688.94   7.693    772
    687.31   7.675    147
    685.69   7.657     91
    683.56   7.633     75
    681.63   7.611     76
    680.38   7.597     43
    679.56   7.588     69
    675.19   7.539    180
    674.06   7.527    192
    673.13   7.516    262
    671.06   7.493    885
    670.50   7.487   1000
    668.75   7.468    989
    668.19   7.461    750
    665.88   7.436    366
    665.25   7.428    442
    664.56   7.421    432
    663.50   7.409    516
    662.38   7.396    143
    660.00   7.370     96
    658.75   7.356    168
    657.50   7.342     76
    656.25   7.328     65
    655.13   7.315     48
    654.19   7.305     60

in CDCl3