116-29-0

三氯杀螨砜(116-29-0)质谱(MS)

产品名称:三氯杀螨砜

CAS:116-29-0

分子式:C12H6Cl4O2S

分子量: 356.05

Mass

MS-NW-7324          
p-chlorophenyl 2,4,5-trichlorophenyl sulfone
C12H6Cl4O2S         (Mass of molecular ion:    354)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      39.0       1.0
      45.0       1.2
      50.0      10.8
      51.0       5.8
      61.0       1.9
      62.0       1.6
      63.0       2.4
      69.0       1.5
      73.0       5.1
      74.0      14.3
      75.0      35.5
      76.0       7.1
      79.0       1.6
      84.0       4.6
      85.0       5.1
      86.0       1.7
      87.0       2.2
      96.0       1.0
      97.0       2.0
      99.0      10.5
     101.0       3.2
     107.0       1.2
     108.0       7.1
     109.0       8.8
     110.0       4.1
     111.0      72.2
     112.0       5.5
     113.0      22.3
     114.0       1.8
     127.0      33.0
     128.0       3.1
     129.0      11.1
     131.0       5.8
     133.0       2.3
     143.0       9.0
     144.0       5.9
     145.0      10.0
     146.0       9.5
     147.0       4.1
     148.0       1.7
     150.0       1.8
     159.0     100.0
     160.0       8.1
     161.0      37.4
     162.0       3.0
     163.0       1.9
     167.0       1.7
     169.0       1.6
     175.0      18.8
     176.0       2.7
     177.0       7.1
     178.0       1.7
     179.0       6.9
     180.0       1.1
     181.0       6.1
     183.0       2.4
     184.0       2.0
     185.0       1.4
     195.0       1.9
     197.0       1.3
     199.0       2.3
     201.0       2.0
     220.0       5.2
     221.0       1.0
     222.0       3.3
     227.0      53.6
     228.0       4.3
     229.0      54.7
     230.0       4.3
     231.0      19.1
     232.0       1.5
     233.0       2.6
     236.0       1.2
     254.0       2.2
     255.0       1.4
     256.0       2.0
     257.0       1.1
     290.0       1.4
     292.0       1.7
     354.0      32.3
     355.0       5.8
     356.0      42.4
     357.0       6.6
     358.0      21.9
     359.0       3.3
     360.0       5.3

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₂ H₆ Cl₄ O₂ S	0.046 g : 0.5 ml CDCl₃
p-chlorophenyl 2,4,5-trichlorophenyl sulfone

    Assign.     Shift(ppm)

      A             8.415
      B             7.89
      C             7.55
      D             7.51
     
     J(A,C)=0.3HZ.

     Hz     ppm     Int.

    753.81   8.417    719
    714.00   7.973     39
    711.63   7.946    374
    709.50   7.923    123
    704.88   7.871    146
    702.69   7.847    574
    700.44   7.821     83
    678.81   7.580     88
    678.06   7.572     38
    676.19   7.551   1000
    674.38   7.530    169
    669.75   7.479    119
    667.63   7.455    363
    665.31   7.429     40

in CDCl3