17228-64-7

2-氯-6-甲氧基吡啶(17228-64-7)质谱(MS)

产品名称:2-氯-6-甲氧基吡啶

CAS:17228-64-7

分子式:C6H6ClNO

分子量: 143.57

InChI:InChI=1S/C6H6ClNO/c1-9-6-4-2-3-5(7)8-6/h2-4H,1H3

InChIKey: VAVGOGHLNAJECD-UHFFFAOYSA-N

Smiles:C1(Cl)=NC(OC)=CC=C1

Mass

MS-NW-1318          
2-chloro-6-methoxypyridine
C6H6ClNO            (Mass of molecular ion:    143)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       7.5
      18.0       1.4
      26.0       4.4
      27.0       3.5
      28.0       5.2
      29.0       2.8
      32.0       1.3
      36.0       1.1
      37.0       8.8
      38.0      20.6
      39.0      38.9
      40.0       2.1
      42.0       1.1
      47.0       1.2
      49.0       3.6
      50.0      10.5
      51.0      11.7
      52.0       5.4
      53.0       4.9
      54.0       1.0
      60.0       1.6
      61.0       1.7
      62.0       2.2
      63.0       2.8
      64.0      11.8
      65.0      12.8
      66.0       3.2
      67.0       1.0
      73.0       3.3
      74.0       1.9
      75.0       3.9
      76.0      14.8
      77.0       6.9
      78.0      79.4
      79.0       7.7
      80.0       3.7
      85.0       3.2
      86.0       4.4
      87.0       1.5
      88.0       1.4
      93.0      17.5
      94.0       2.9
     100.0       5.1
     102.0       2.1
     106.0       3.2
     107.0       1.0
     108.0      11.2
     109.0       3.7
     110.0       1.6
     112.0       9.9
     113.0      78.0
     114.0      36.6
     115.0      27.3
     116.0      11.1
     138.0       5.2
     139.0       5.9
     140.0       1.4
     142.0     100.0
     143.0      83.7
     144.0      36.5
     145.0      26.3
     146.0       1.9

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₆ Cl N O	0.04 ml : 0.5 ml CDCl₃
2-chloro-6-methoxypyridine

    Assign.     Shift(ppm)

      A             7.50
      B             6.89
      C             6.65
      D             3.93

     Hz     ppm     Int.

    679.31   7.585     69
    671.81   7.502     98
    671.19   7.495     91
    663.69   7.411    106
    620.06   6.924    105
    619.38   6.916    112
    612.63   6.841     86
    611.88   6.833     81
    598.75   6.686    111
    598.06   6.678    101
    590.63   6.595     88
    589.94   6.588     82
    351.81   3.929   1000

in CDCl3