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ChemicalBook CAS DataBase List [1,1'-Biphenyl]-3-methanamine, 2-methyl-

[1,1'-Biphenyl]-3-methanamine, 2-methyl- synthesis

3synthesis methods
76350-90-8 Synthesis
2-Methyl-3-biphenylmethanol

76350-90-8
244 suppliers
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[1,1'-Biphenyl]-3-methanamine, 2-methyl-

1061650-37-0
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere
2.1: ethanol; hydrazine hydrate monohydrate / 3 h / Reflux
2.2: 0.5 h / Reflux

References:

WO2022/33303,2022,A1