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ChemicalBook CAS DataBase List 1,1-DIBROMO-1-PROPENE

1,1-DIBROMO-1-PROPENE synthesis

12synthesis methods
-

Yield:13195-80-7 80%

Reaction Conditions:

Stage #1: carbon tetrabromidewith triphenylphosphine;zinc in dichloromethane at 23; for 0.5 h;Inert atmosphere;
Stage #2: acetaldehyde at 0; for 0.5 h;

References:

Newcomb, Eric T.;Knutson, Phil C.;Pedersen, Blaine A.;Ferreira, Eric M. [Journal of the American Chemical Society,2016,vol. 138,# 1,p. 108 - 111] Location in patent:supporting information

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