1,10-BIS(TRICHLOROSILYL)DECANE, tech-95 synthesis
- Product Name:1,10-BIS(TRICHLOROSILYL)DECANE, tech-95
- CAS Number:52217-62-6
- Molecular formula:C10H20Cl6Si2
- Molecular Weight:409.15
2162-98-3
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52217-62-6
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Yield:52217-62-6 74.8%
Reaction Conditions:
with trichlorosilane;tetra-n-butylphosphonium chloride at 150; for 6 h;Inert atmosphere;Sealed tube;
Steps:
15 Example 4: Reaction of chloroform and trichlorosilane (Catalyst: a catalyst in which tetrabutylphosphonium chloride immobilizedto chloropropyl Silsesquioxane)
General procedure: In the ovenDriedNitrogen gas in a stainless steel high pressure reactor with a capacity of 75 millilitersUnder0.4 g (0.16 mmol)And tributylphosphine immobilized on chloropropyl silsesukuoxen15 g (0.13 mol) of chloroform and 52.8 g(0.39 mol) of trichlorosilane was added. Seal the reactorAfter reacting at 150 for 2 hours, the reactant was distilled under reduced pressure.18.9 g (yield 51.3%) of bis (trichlorosilyl) methane was obtained
References:
KR2020/15644,2020,A Location in patent:Paragraph 0056-0057; 0100-0102
1647-16-1
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10025-78-2
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52217-62-6
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