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1,2,2,2-TETRACHLORO-1-FLUOROETHYL METHYL ETHER synthesis

1synthesis methods
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Yield:37021-34-4 42%

Reaction Conditions:

Stage #1: methoxyfluranewith potassium hydroxideHeating;Dehydrofluorination;
Stage #2: with chlorine at -40;Chlorination;

References:

Ramig, Keith;Kudzma, Linas V.;Lessor, Ralph A.;Rozov, Leonid A. [Journal of Fluorine Chemistry,1999,vol. 94,# 1,p. 1 - 5]

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