1-(2,4-DIETHOXY-PHENYL)-ETHANONE synthesis
- Product Name:1-(2,4-DIETHOXY-PHENYL)-ETHANONE
- CAS Number:22924-18-1
- Molecular formula:C12H16O3
- Molecular Weight:208.25
19074-30-7
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$110.00/50mg
75-05-8
1015 suppliers
$10.00/10g
22924-18-1
58 suppliers
$45.00/50mg
Yield:22924-18-1 74%
Reaction Conditions:
Stage #1: 2,4-diethoxybenzoic acid;acetonitrilewith palladium(II) trifluoroacetate;6-methyl-2,2'-bipyridine in water at 130; for 1 h;Microwave irradiation;
Stage #2: with formic acid in water at 100; for 1 h;
References:
Lindh, Jonas;Sjoeberg, Per J. R.;Larhed, Mats [Angewandte Chemie - International Edition,2010,vol. 49,# 42,p. 7733 - 7737] Location in patent:supporting information; experimental part
89-84-9
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75-03-6
364 suppliers
$11.00/5g
22924-18-1
58 suppliers
$45.00/50mg
37470-42-1
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$450.00/1g
2049-73-2
88 suppliers
$26.67/10g
75-36-5
589 suppliers
$17.92/100G
22924-18-1
58 suppliers
$45.00/50mg