1-(2-chloropropoxy)-2-(phenylmethyl)benzene synthesis
- Product Name:1-(2-chloropropoxy)-2-(phenylmethyl)benzene
- CAS Number:85909-36-0
- Molecular formula:C16H17ClO
- Molecular Weight:260.7586
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Yield:85909-36-0 88.59%
Reaction Conditions:
with Dichloromethylsilane;iron(III) chloride in 1,2-dimethoxyethane at 84; for 4 h;Reflux;Green chemistry;
Steps:
3 Example 3: (2-Benzylphenyl)2-chloropropyl ether
In a 500 ml three-necked flask, Compound B (23.5 g, 103 mmol), methyldichlorosilane (14.22 g, 123.6 mmol), anhydrous ferric chloride (1.67 g, 10.3 mmol), and ethylene glycol dimethyl ether 200 ml were added. The reaction solvent was heated to reflux at 84 ° C for 4 hours. After completion of the reaction, the solvent was removed under reduced pressure and dried.Recrystallization from ethyl acetate gave a white solid C (23.8 g).The yield was 88.59%.
References:
CN108752290,2018,A Location in patent:Paragraph 0022; 0023; 0024
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