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ChemicalBook CAS DataBase List 1,2-Di(4-carboxyphenyl)-1,2-diphenylethylene

1,2-Di(4-carboxyphenyl)-1,2-diphenylethylene synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: zinc; titanium tetrachloride / tetrahydrofuran / 6 h / -5 - 75 °C / Inert atmosphere
2.1: tetrahydrofuran / 72 h / 160 °C
2.2: 3 h / Reflux
3.1: sodium hydroxide / ethylene glycol / 72 h / 200 °C

References:

Liu, Xun-Gao;Tao, Chen-Lei;Yu, Huang-Qin;Chen, Bin;Liu, Zhen;Zhu, Gen-Ping;Zhao, Zujin;Shen, Liang;Tang, Ben Zhong [Journal of Materials Chemistry C,2018,vol. 6,# 12,p. 2983 - 2988]

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