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ChemicalBook CAS DataBase List 1,2-Dioleoyl-sn-glycero-3-phosphoethanolamine

1,2-Dioleoyl-sn-glycero-3-phosphoethanolamine synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 84 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / CH2Cl2; H2O / 2 h
2: 1) Et3N, POCl3, 2) Et3N / 1) THF, a) 0 deg C, 1 h, b) room temp., 3 h, 2) THF, a) 0 deg C, 4 h, b) room temp., 8 h

References:

Lebeau, Luc;Oudet, Pierre;Mioskowski, Charles [Helvetica Chimica Acta,1991,vol. 74,# 8,p. 1697 - 1706]

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