
1, 2-Epoxyucyclohex-4-ene synthesis
- Product Name:1, 2-Epoxyucyclohex-4-ene
- CAS Number:6253-27-6
- Molecular formula:C6H8O
- Molecular Weight:96.13
Yield:71-43-2 51 %Chromat. ,6253-27-6 49 %Chromat.
Reaction Conditions:
with [(N-benzenesulfonyl-N,N’-bis(2-pyridylmethyl)-1,2-cyclohexanediamine)-diacetonitrilocobalt(II)] perchlorate;3-chloro-benzenecarboperoxoic acid in acetonitrile at 24.84; for 0.5 h;Catalytic behavior;Reagent/catalyst;
Steps:
Reactivity
General procedure: Unless stated otherwise, all reactivity studies were done at 298 K in MeCN under air. The yields of organic products were determined by GC; all reported values are the average of the measurements for at least three independent reactions. The listed errors represent one standard deviation. The identities and yields of products were confirmed by comparing the GC retention times with those of authentic compounds and by comparing the peak integrations with that of a non-reactive 1,2-dichlorobenzene internal standard
References:
Bell-Taylor, Angela;Gorden, John D.;Hardy, Emily E.;Goldsmith, Christian R. [Inorganica Chimica Acta,2018,vol. 482,p. 206 - 212]

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