1,3,6-HEXANETRICARBONITRILE synthesis
- Product Name:1,3,6-HEXANETRICARBONITRILE
- CAS Number:1772-25-4
- Molecular formula:C9H11N3
- Molecular Weight:161.2
107-13-1
434 suppliers
$17.00/25ML
2941-23-3
163 suppliers
$7.00/1g
1772-25-4
151 suppliers
$45.00/50mg
Yield:1772-25-4 66.9%
Reaction Conditions:
with sodium hydroxide in toluene;
Steps:
6 Example 6
Example 6 Production of 1,3,6-hexanetricarbonitrile by isolating 2-amino-1 -cyclopentene-1 -carbonitrile 583 mg (11 mmol) of acrylonitrile were added at room temperature to a mixture of 1.08 g (10 mmol) of 2-amino-1-cyclopentene-1-carbonitrile (from Example 5), 2 ml (33.7 mmol) of 45% sodium hydroxide solution, 100 mg of Aliquat 336 and 6 ml of toluene and stirred at 50° C. for 22 hours. The mixture was diluted with water, the phases were separated, the organic phase was dried, the solvent was distilled off and the residue was examined by gas chromatography. Trimer yield: 66.9%
References:
US2002/7081,2002,A1
111-69-3
197 suppliers
$14.00/25mL
865-47-4
711 suppliers
$14.00/25g
107-13-1
434 suppliers
$17.00/25ML
1772-25-4
151 suppliers
$45.00/50mg
111-69-3
197 suppliers
$14.00/25mL
107-13-1
434 suppliers
$17.00/25ML
1772-25-4
151 suppliers
$45.00/50mg
141-28-6
375 suppliers
$10.00/100g
1772-25-4
151 suppliers
$45.00/50mg
111-69-3
197 suppliers
$14.00/25mL
1772-25-4
151 suppliers
$45.00/50mg