1,3-Benzodioxole-4-carboxylic acid, 5-formyl- synthesis
- Product Name:1,3-Benzodioxole-4-carboxylic acid, 5-formyl-
- CAS Number:58343-48-9
- Molecular formula:C9H6O5
- Molecular Weight:194.14
120-57-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: p-toluenesulfonic acid / methanol / 1 h / Heating
2: 1) n-butyllithium / 1) ether, ice-water cooling, 1 h, 2) dry ice-acetone bath
References:
Napolitano, Elio;Giannone, Enrico;Fiaschi, Rita;Marsili, Antonio [Journal of Organic Chemistry,1983,vol. 48,# 21,p. 3653 - 3657]
![5-DIMETHOXYMETHYL-BENZO[1,3]DIOXOLE](/CAS/GIF/59259-90-4.gif)
